UHPLC-HRMS quality parameters for the analysis of PLTX samples (System I, Method 1, QM-B).
Concentration | % | |
---|---|---|
Run-to-run precision (RSD, %) | Low level (75 ng mL−1) | 1.3 |
Medium level (800 ng mL−1) | 1.0 | |
Day-to-day precision (RSD, %) | Low level (75 ng mL−1) | 1.6 |
Medium level (800 ng mL−1) | 3.4 | |
Trueness (rel. error, %) | Low level (75 ng mL−1) | 7.6 |
Medium level (800 ng mL−1) | 9.7 | |
LOQ | 6.5 ng mL−1 |