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. 2023 Oct 31;8(45):42356–42366. doi: 10.1021/acsomega.3c04656

Table 2. 13C NMR Data of Isolated Compounds in Pyridine.

  3 9 7 8
position cucurbitacin E cucurbitacin E 2-O-β-d-glucopyranoside neocucurbitan A neocucurbitan B
1 115.8, CH 121.3, CH 134.3, CH 134.4, CH
2 147.3, C 145.3, C    
3 199.0, C 198.9, C 172.6, C 172.6, C
4 48.6, C 48.9, C 42.6, C 42.6, C
5 137.7, C 135.6, C 132.7, C 132.7, C
6 120.5, CH 121.3, CH 123.8, CH 123.8, CH
7 23.9, CH2 23.7, CH2 25.0, CH2 25.0, CH2
8 42.1, CH 41.3, CH 42.4, CH 42.3, CH
9 49.3, C 48.9, C 47.9, C 47.8, C
10 35.1, CH 35.4, CH 117.7, C 117.6, C
11 213.8, C 214.6, C 211.9, C 211.8, C
12 49.3, CH2 49.0, CH2 50.4, CH2 50.5, CH2
13 48.6, C 50.6, C 48.9, C 51.0, C
14 51.0, C 48.0, C 51.0, C 48.9, C
15 46.5, CH2 45.5, CH2 45.7, CH2 45.8, CH2
16 70.7, CH 71.2, CH 70.4, CH 70.2, CH
17 60.0, CH 58.2, CH 59.8, CH 59.3, CH
18 20.6, CH3 20.2, CH3 20.4, CH3 20.4, CH3
19 20.1, CH3 20.0, CH3 25.1, CH3 25.2, CH3
20 79.8, C 78.2, C 79.6, C 79.2, C
21 25.6, CH3 24.0, CH3 25.4, CH3 25.4, CH3
22 204.4, C 202.6, C 204.2, C 204.2,C
23 122.5, CH 120.4, CH 122.4, CH 120.8, CH
24 150.2, CH 152.0, CH 150.3, CH 155.7, CH
25 79.7, C 79.4, C 79.8, C 70.2, C
26 26.2, CH3 25.9, CH3 26.2, CH3 29.7, CH3
27 26.5, CH3 26.5, CH3 26.6, CH3 30.0, CH3
28 18.4, CH3 19.9, CH3 18.1, CH3 18.0, CH3
29 28.0, CH3 27.9, CH3 28.5, CH3 22.4, CH3
30 20.8, CH3 18.2, CH3 22.3, CH3 28.5, CH3
31 169.8, C 170.4, C 169.8, C  
32 21.7, CH3 22.0, CH3 21.7, CH3  
1′-Oglc   100.5, CH    
2′   72.3, CH    
3′   75.8, CH    
4′   69.3, CH    
5′   76.7, CH    
6′   61.5, CH2