Table 1.
X-ray data collection and refinement statistics
| GDNF10 – GFRα110 (PDB code: 8OS6) | |
|---|---|
| Resolution range | 85.02–2.65 (2.70–2.65) |
| Space group | P21 |
| Unit cell (a,b,c, α,β,γ) | 114.1 170.0 130.8 90 96.2 90 |
| Total reflections | 1898819 (80645) |
| Unique reflections | 140996 (6703) |
| Multiplicity | 13.5 (12.0) |
| Completeness (%) | 99.1 (95.5) |
| Mean I/sigma(I) | 4.75 (0.25) |
| Wilson B-factor | 57.69 |
| R-pim | 0.1078 (4.085) |
| CC1/2 | 0.990 (0.281) |
| CC* | 0.996 (0.691) |
| Reflections used in refinement | 125,175 (4121) |
| Reflections used for R-free | 6139 (195) |
| R-work | 0.2383 (0.5179) |
| R-free | 0.2797 (0.5074) |
| CC(work) | 0.929 (0.627) |
| CC(free) | 0.929 (0.567) |
| Number of non-hydrogen atoms | 23835 |
| macromolecules | 23416 |
| ligands | 689 |
| solvent | 19 |
| Protein residues | 3001 |
| RMS(bonds) | 0.002 |
| RMS(angles) | 0.47 |
| Ramachandran favoured (%) | 96.48 |
| Ramachandran allowed (%) | 3.49 |
| Ramachandran outliers (%) | 0.03 |
| Rotamer outliers (%) | 3.50 |
| Clashscore | 4.80 |
| Average B-factor | 82.70 |
| macromolecules | 82.57 |
| ligands | 90.75 |
| solvent | 70.04 |
| Number of TLS groups | 108 |
Statistics for the highest-resolution shell are shown in parentheses.