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. 2023 Nov 23;13:20612. doi: 10.1038/s41598-023-46841-2

Table 1.

DEPT-Q (400 MHz) and 1H (100 MHz) NMR data of compounds 1, 2, 3 in DMSO-d6; Carbon multiplicities were determined by the DEPT-Q experiments.

Nu 1 2 3
δC δH (J in Hz) δC δH (J in Hz) δC δH (J in Hz)
1 38.6, CH2 0.87, 1.58, m 38.5, CH2 0.87, 1.58, m 38.6, CH2 0.87, 1.58, m
2 26.2, CH2 1.52, 1.70, m 26.2, CH2 1.52, 1.70, m 26.1, CH2 1.52, 1.70, m
3 87.4, CH 3.00, m 87.5, CH 3.00, m 87.5, CH 3.00, m
4 37.2, qC 37.0, qC 37.2, qC
5 55.7, CH 0.69, m 55.7, CH 0.69, m 55.5, CH 0.69, m
6 17.8, CH2 1.09, 1.45, m 17.8, CH2 1.09, 1.45, m 17.8, CH2 1.09, 1.45, m
7 35.5, CH2 1.36, 1.44, m 35.5, CH2 1.36, 1.44, m 35.5, CH2 1.36, 1.44, m
8 36.8, qC 36.9, qC 36.8, qC
9 52.3, CH 0.80, s 52.3, CH 0.80, s 52.3, CH 0.80, s
10 36.8, qC 36.9, qC 36.8, qC
11 22.6, CH2 1.33, 1.49, m 22.6, CH2 1.33, 1.49, m 22.6, CH2 1.33, 1.49, m
12 27.8, CH2 1.56, 1.72, m 27.9, CH2 1.56, 1.72, m 27.9, CH2 1.56, 1.72, m
13 36.1, CH 1.01, m 36.0, CH 1.01, m 36.1, CH 1.01, m
14 52.7, qC 52.9, qC 52.7, qC
15 36.2, CH2 1.89, 2.38, s 36.0, CH2 1.89, 2.38, s 36.0, CH2 1.89, 2.38, s
16 109.5, qC 109.7, qC 109.3, qC
17 53.1, CH 0.84, s 53.0, CH 0.84, s 53.0, CH 0.84, s
18 18.9, CH3 1.03, s 18.9, CH3 1.03, s 18.9, CH3 1.03, s
19 16.5, CH3 0.77, s 16.6, CH3 0.77, s 16.5, CH3 0.77, s
20 67.5, qC 67.7, qC 67.5, qC
21 29.7, CH3 1.03, s 29.7, CH3 1.03, s 29.7, CH3 1.03, s
22 44.4, CH2 1.24, 1.36, m 44.4, CH2 1.24, 1.36, m 44.5, CH2 1.24, 1.36, m
23 67.4, CH 4.48, m 67.4, CH 4.48, m 67.4, CH 4.48, m
24 126.1, CH 5.08, d, (8.0) 126.1, CH 5.08, d, (8.0) 126.3, CH 5.08, d, (8,0)
25 133.6, qC 133.8, qC 133.6, qC
26 18.6, CH3 1.60, s 18.6, CH3 1.60, s 18.6, CH3 1.60, s
27 25.7, CH3 1.65, s 25.7, CH3 1.65, s 25.8, CH3 1.65, s
28 27.6, CH3 0.89, s 27.6, CH3 0.89, s 27.6, CH3 0.89, s
29 16.4, CH3 0.68, s 16.4, CH3 0.68, s 16.4, CH3 0.68, s
30 65.4, CH2 3.41, 3.67, s 65.4, CH2 3.41, 3.67, s 65.3, CH2 3.41, 3.67, s

qC quaternary, CH methine, CH2 methylene, CH3 methyl carbons.