Table 1.
Nu | 1 | 2 | 3 | |||
---|---|---|---|---|---|---|
δC | δH (J in Hz) | δC | δH (J in Hz) | δC | δH (J in Hz) | |
1 | 38.6, CH2 | 0.87, 1.58, m | 38.5, CH2 | 0.87, 1.58, m | 38.6, CH2 | 0.87, 1.58, m |
2 | 26.2, CH2 | 1.52, 1.70, m | 26.2, CH2 | 1.52, 1.70, m | 26.1, CH2 | 1.52, 1.70, m |
3 | 87.4, CH | 3.00, m | 87.5, CH | 3.00, m | 87.5, CH | 3.00, m |
4 | 37.2, qC | 37.0, qC | 37.2, qC | |||
5 | 55.7, CH | 0.69, m | 55.7, CH | 0.69, m | 55.5, CH | 0.69, m |
6 | 17.8, CH2 | 1.09, 1.45, m | 17.8, CH2 | 1.09, 1.45, m | 17.8, CH2 | 1.09, 1.45, m |
7 | 35.5, CH2 | 1.36, 1.44, m | 35.5, CH2 | 1.36, 1.44, m | 35.5, CH2 | 1.36, 1.44, m |
8 | 36.8, qC | 36.9, qC | 36.8, qC | |||
9 | 52.3, CH | 0.80, s | 52.3, CH | 0.80, s | 52.3, CH | 0.80, s |
10 | 36.8, qC | 36.9, qC | 36.8, qC | |||
11 | 22.6, CH2 | 1.33, 1.49, m | 22.6, CH2 | 1.33, 1.49, m | 22.6, CH2 | 1.33, 1.49, m |
12 | 27.8, CH2 | 1.56, 1.72, m | 27.9, CH2 | 1.56, 1.72, m | 27.9, CH2 | 1.56, 1.72, m |
13 | 36.1, CH | 1.01, m | 36.0, CH | 1.01, m | 36.1, CH | 1.01, m |
14 | 52.7, qC | 52.9, qC | 52.7, qC | |||
15 | 36.2, CH2 | 1.89, 2.38, s | 36.0, CH2 | 1.89, 2.38, s | 36.0, CH2 | 1.89, 2.38, s |
16 | 109.5, qC | 109.7, qC | 109.3, qC | |||
17 | 53.1, CH | 0.84, s | 53.0, CH | 0.84, s | 53.0, CH | 0.84, s |
18 | 18.9, CH3 | 1.03, s | 18.9, CH3 | 1.03, s | 18.9, CH3 | 1.03, s |
19 | 16.5, CH3 | 0.77, s | 16.6, CH3 | 0.77, s | 16.5, CH3 | 0.77, s |
20 | 67.5, qC | 67.7, qC | 67.5, qC | |||
21 | 29.7, CH3 | 1.03, s | 29.7, CH3 | 1.03, s | 29.7, CH3 | 1.03, s |
22 | 44.4, CH2 | 1.24, 1.36, m | 44.4, CH2 | 1.24, 1.36, m | 44.5, CH2 | 1.24, 1.36, m |
23 | 67.4, CH | 4.48, m | 67.4, CH | 4.48, m | 67.4, CH | 4.48, m |
24 | 126.1, CH | 5.08, d, (8.0) | 126.1, CH | 5.08, d, (8.0) | 126.3, CH | 5.08, d, (8,0) |
25 | 133.6, qC | 133.8, qC | 133.6, qC | |||
26 | 18.6, CH3 | 1.60, s | 18.6, CH3 | 1.60, s | 18.6, CH3 | 1.60, s |
27 | 25.7, CH3 | 1.65, s | 25.7, CH3 | 1.65, s | 25.8, CH3 | 1.65, s |
28 | 27.6, CH3 | 0.89, s | 27.6, CH3 | 0.89, s | 27.6, CH3 | 0.89, s |
29 | 16.4, CH3 | 0.68, s | 16.4, CH3 | 0.68, s | 16.4, CH3 | 0.68, s |
30 | 65.4, CH2 | 3.41, 3.67, s | 65.4, CH2 | 3.41, 3.67, s | 65.3, CH2 | 3.41, 3.67, s |
qC quaternary, CH methine, CH2 methylene, CH3 methyl carbons.