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. 2023 Nov 10;9(11):2161–2170. doi: 10.1021/acscentsci.3c01087

Table 2. Representative Conditions for the Microwave-Assisted Synthesis of High-Crystallinity MOF-322.

Exp. H2TVDC (mmol) Al3+ (mmol) OH– (mmol) H2O (mL) Time (min) Temp. (°C)
22 1.0 0.46 2.0 3.6 40 145
68 1.0 0.21 1.75 1.5 35 145
86 1.0 0.41 1.5 4.3 40 150
103 1.0 0.46 2.0 3.4 60 140
109 1.0 0.99 2.0 3.5 50 150