Table 1.
Quantification of reagents, solvent, and product
| Reagent | Mw (g/mol) | m (mg) | n (mmol) | Equiv. | V (mL) | Conc (M) | Yield (%) |
|---|---|---|---|---|---|---|---|
| 1 | 220 | 44 | 0.2 | 1 | 0.4 | ||
| Mn(CO)5Br | 274 | 1.0 | 0.004 | 0.02 | |||
| SL1 | 773 | 3.4 | 0.0044 | 0.022 | |||
| 15-crown-5 | 0.5 | ||||||
| tBuOK | 112 | 4.5 | 0.04 | 0.2 | |||
| (2R, 3S)-2 | 224 | 42 | 0.19 | 95 |