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. Author manuscript; available in PMC: 2024 Jun 20.
Published in final edited form as: Biochemistry. 2023 Jun 7;62(12):1964–1975. doi: 10.1021/acs.biochem.3c00083

Table 2.

g values and relative contributions from the crosslinked and non-crosslinked protein fractions obtained from fits of the EPR spectra shown in Figures 4, 5, and S3–S5

Sample Species % Contribution g1 g2 g3
A. WT MmCDO Prep 1 Crosslinked 65 2.378 2.235 1.935
Non-crosslinked 35 2.335 2.205 1.951
B. WT MmCDO Prep 2 Crosslinked 88 2.378 2.235 1.935
Non-crosslinked 12 2.335 2.205 1.951
C. C93G MmCDO Non-crosslinked 100 2.349 2.243 1.941
D. WT BsCDO Non-crosslinked 100 2.327 2.227 1.948
E. G82C BsCDO
High Iron Prep 1		 Crosslinked 79 2.370 2.223 1.935
Non-crosslinked 21 2.326 2.223 1.949
F. G82C BsCDO
Low Iron Prep 4		 Crosslinked 67 2.370 2.223 1.939
Non-crosslinked 33 2.326 2.223 1.949