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. 2023 Nov 10;14(47):13799–13811. doi: 10.1039/d3sc04183b

Photoconversion parameters of NPy-Aa-d, NPy-S, and CPy-S. σI, σII, and σIII, respectively denote the uncaging cross-sections of the caged pyranine derivatives extracted from analyzing (i) the time dependence of the rise of the fluorescence emission at 540 nm for solutions of NPy-Aa-d, at 500 nm for the solution of NPy-S, and at 510 nm for the solution of CPy-S under monochromatic illumination at 365 nm; (ii) the light intensity-dependence of the inverse of the associated characteristic time τ for NPy-Ab, NPy-Ad, NPy-S and CPy-S at 365 nm; (iii) the time evolution of the concentrations in caged pyranine derivative and its photoreleased free pyranine derivative measured by capillary electrophoresis (for NPy-Ab) and HPLC (for NPy-Ad, NPy-S and CPy-S) under illumination at 365 nm. T = 293 K.

Pyranine derivatives σ I (m2 mol−1) σ II (m2 mol−1) σ III (m2 mol−1)
NPy-Aa 1.6 ± 0.2
NPy-Ab 6.8 ± 0.7 6.2 ± 0.6 8.2 ± 0.8
NPy-Ac 18.3 ± 2.0
NPy-Ad 15.6 ± 1.6 38.9 ± 3.9 25.2 ± 2.5
NPy-S 8.4 ± 0.7 16.3 ± 1.6 6.0 ± 0.6
CPy-S 560 ± 56 462 ± 46 695 ± 70