Thermal properties of polysaccharides before and after UO22+ adsorptiona.
| Step | G | U–G | ||||
|---|---|---|---|---|---|---|
| Onset temp. (°C) | DTG (°C) | Wt loss (%) | Onset temp. (°C) | DTG (°C) | Wt loss (%) | |
| Step 1 | — | 73.55 | 6.02 | — | 79.01 | 3.85 |
| Step 2 | 149.61 | 314.90 | 80.66 | 166.75 | 268.91 | 37.93 |
| Step 3 | — | — | — | 318.06 | 334.20 | 20.43 |
| 404.85 | ||||||
| Residue | 13.31 | 37.75 | ||||
| X | U–X | |||||
| Step 1 | — | 114.64 | 4.36 | — | 68.85 | 6.23 |
| Step 2 | 176.84 | 275.17 | 65.68 | 154.65 | 273.19 | 33.55 |
| Step 3 | — | — | — | 350.34 | 348.39 | 11.07 |
| Step 4 | — | — | — | 600.5 | 857.25 | 6.04 |
| Residue | 29.94 | 43.14 | ||||
| I | U–I | |||||
| Step 1 | — | 87.44 | 6.92 | — | 71.49 | 9.67 |
| Step 2 | 137.24 | 164.84 | 25.02 | 156.67 | 222.92 | 18.59 |
| Step 3 | 184.98 | 256.15 | 12.81 | 300.91 | 356.73 | 6.87 |
| Step 4 | 307.36 | 351.05 | 12.11 | 393.72 | 443.93 | 10.29 |
| Step 5 | 599.95 | 747.71 | 16.61 | 509.72 | 601.06 | 13.26 |
| Residue | 26.54 | 37.05 | ||||
| K | U–K | |||||
| Step 1 | — | 69.19 | 9.31 | — | 76.24 | 7.07 |
| Step 2 | 146.58 | 259.39 | 22.39 | 156.67 | 278.44 | 28.40 |
| Step 3 | 277.71 | 321.94 | 23.10 | 395.73 | 440.94 | 22.82 |
| Step 4 | 500.64 | 747.92 | 17.04 | — | — | — |
| Residue | 28.16 | 41.72 | ||||
Sorption conditions: 700 mg per L UO22+, 3 mL of 1% w/v polysaccharide.