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. 2023 Sep 29;15(1):195–203. doi: 10.1039/d3sc01944f

Scope and optimization of Fmoc-arylglycine incorporation in SPPS. Experimental protocol: Fmoc removal: 1% DBU in DMF, 3 × 30 s, RT and coupling: Fmoc-AA-OH, DIC, Oxyma, DMF (for time and temperature see Table).

graphic file with name d3sc01944f-u1.jpg
a

Calculated by chiral RP-HPLC UV spectra at 254 nm. ch: conventional heating.