TABLE 4.

¹H NMR data for F. meningosepticum phosphoryl-methylated lipid A^a

Proton	Value for chemical shift (ppm)
	GlcN I	Fatty acid
H-1	6.01b
H-2	4.68
H-3	5.64
H-4	3.98
H-5	4.19
H-6a	4.39
H-6b	4.10
2-NH	8.12
4-OH	5.86
Hα1		2.53
Hα2		2.58
Hα3		2.69
Hα4		2.79
Hβ1		4.19
Hβ2		4.27
Hβ3		4.28
Hβ4		5.64
Hβ1-OH		4.82
Hβ2-OH		4.92
Hβ3-OH		4.96

^aSpectra were recorded at 600 MHz in C₆D₆–(CD₃)₂ SO (9:1) relative to TMS (0.00 ppm). Assignments were made by field gradient ¹H,¹H-COSY NMR. Chemical shifts for the nonreducing terminal unit were not clearly assigned because of heterogeneity. 

^bJ = 3.12 Hz.