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. 2023 Sep 20;20:100890. doi: 10.1016/j.fochx.2023.100890

Table 1.

Identified wax constituents in C. aurantium L. fruit peel extract, their retention times (min) and relative concentrations (a relative percentage of the area of peaks, %) in each peel sample (HN, JX, JY, and SC).

Retention times (min) Waxes HN (%) JX (%) JY (%) SC (%)
10.283 Dodecanoic acid 0.06 ± 0.00 0.10 ± 0.01 0.12 ± 0.04 0.10 ± 0.01
12.285 Methyl hexadecanoate 0.13 ± 0.03 0.19 ± 0.02 0.25 ± 0.06 0.10 ± 0.04
12.399 Pentadecanoic acid 0.22 ± 0.08 0.40 ± 0.08 0.51 ± 0.15 0.15 ± 0.04
12.723 Ethyl hexadecanoate 0.01 ± 0.00 0.04 ± 0.02 0.31 ± 0.17 0.04 ± 0.03
12.884 9-Hexadecenoic acid 0.15 ± 0.04 0.22 ± 0.01 0.36 ± 0.06 0.14 ± 0.01
13.384 Methyl 10-trans,12-cis-octadecadienoate 0.01 ± 0.00 0.03 ± 0.01 0.12 ± 0.05 0.02 ± 0.01
13.424 Methyl linolenate 0.01 ± 0.00 0.02 ± 0.01 0.09 ± 0.04 0.02 ± 0.00
13.654 Heptadecanoic acid 0.56 ± 0.02 0.77 ± 0.01 0.94 ± 0.12 0.32 ± 0.11
14.088 Linoleic acid 1.67 ± 0.09 2.27 ± 0.16 2.65 ± 0.04 1.67 ± 0.34
14.265 Stearic acid 1.21 ± 0.06 1.89 ± 0.17 2.05 ± 0.11 1.04 ± 0.29
14.554 11-Methyloctadec-12-enoic acid 0.02 ± 0.00 0.01 ± 0.00 0.02 ± 0.01 0.00 ± 0.00
14.916 Nonadecanoic acid 0.03 ± 0.00 0.06 ± 0.02 0.07 ± 0.01 0.03 ± 0.01
15.481 Oleamide 0.19 ± 0.02 0.07 ± 0.05 0.21 ± 0.05 0.36 ± 0.05
15.682 Eicosanoic acid 0.24 ± 0.03 0.45 ± 0.10 0.45 ± 0.04 0.25 ± 0.08
16.606 Heneicosanoic acid 0.04 ± 0.00 0.08 ± 0.04 0.08 ± 0.01 0.04 ± 0.01
18.941 Geranyl oleate 0.04 ± 0.01 0.04 ± 0.01 0.09 ± 0.05 0.02 ± 0.01
19.366 Butyl linoleate 0.07 ± 0.01 0.07 ± 0.02 0.20 ± 0.08 0.09 ± 0.04
19.445 Oleic anhydride 0.00 ± 0.00 0.00 ± 0.00 0.01 ± 0.00 0.01 ± 0.00
19.520 1-Linolenoylglycerol 0.15 ± 0.04 0.01 ± 0.00 0.03 ± 0.01 0.05 ± 0.02
19.649 2-Methylheptacosane 0.02 ± 0.00 0.05 ± 0.01 0.03 ± 0.00 0.07 ± 0.01
19.981 Trans-13-docosenamide 0.02 ± 0.00 0.01 ± 0.00 0.00 ± 0.00 0.01 ± 0.00
20.334 Octacosane 0.09 ± 0.03 0.15 ± 0.03 0.22 ± 0.05 0.07 ± 0.02
21.018 Lignoceric acid 0.29 ± 0.03 0.44 ± 0.09 0.62 ± 0.20 0.26 ± 0.08
21.860 i-Propyl 24-methyl-pentacosanoate 0.01 ± 0.00 0.01 ± 0.00 0.02 ± 0.01 0.02 ± 0.01
22.046 Citronellyl linoleate 0.02 ± 0.01 0.04 ± 0.01 0.09 ± 0.04 0.01 ± 0.00
22.071 17-Pentatriacontene 0.00 ± 0.00 0.01 ± 0.00 0.02 ± 0.01 0.00 ± 0.00
22.867 Geranyl linoleate 0.01 ± 0.00 0.02 ± 0.01 0.05 ± 0.02 0.00 ± 0.00
22.907 Geranyl palmitoleate 0.00 ± 0.00 0.01 ± 0.00 0.07 ± 0.04 0.00 ± 0.00
23.094 Geranyl linolenate 0.00 ± 0.00 0.01 ± 0.00 0.04 ± 0.03 0.00 ± 0.00
24.393 2,3-Dihydroxypropyl Icosanoate 0.03 ± 0.01 0.01 ± 0.00 0.06 ± 0.02 0.11 ± 0.04
25.974 Ethyl 9,12-hexadecadienoate 0.02 ± 0.00 0.02 ± 0.00 0.03 ± 0.01 0.01 ± 0.00
26.147 1-Heptacosanol 0.06 ± 0.02 0.17 ± 0.02 0.21 ± 0.09 0.09 ± 0.05
28.942 3-Methylhentriacontane 0.00 ± 0.00 0.00 ± 0.00 0.00 ± 0.00 0.01 ± 0.00