Table 2.

Applied drying protocols in the study.

Drying Process	Step	Ts (°C)	Pc (mbar)	Hold Time (h)	Ramp Toward Step (K/min)	MW Application (W)
P1	1	−15	0.05	*	1.0	2 × 90 **
	2	30	0.05	6	1.0	2 × 90 **/†
P2	1	30	0.05	*	0.2
P3	1	30	0.05	*	0.2	2 × 90 ‡
P4	1	10	0.05	*	0.2	2 × 90 §
	2	30	0.05	4	1.0	-

* Maintained until Pirani signal equaled capacitance, and mass spectrometer revealed water vapor concentration c_H2O < 10%. ** In case of MFD. † Applied continuously until the shelf temperature reached 0 °C to not overheat the samples. ‡ Microwave module was stopped after 5 h, 6 h, and 8 h respectively. In case of MFD of F7, 2 × 90 W were applied until Pirani signal equaled capacitance sensor output, and mass spectrometer revealed water vapor concentration c_H2O < 10%. § Microwave module was stopped after 10 h and 13 h, respectively. MW, microwave.