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. 2023 Nov 22;9(12):2277–2285. doi: 10.1021/acscentsci.3c00813

Figure 3.

Figure 3

Reaction optimizations showing total yields for the autoxidation of the acetyl oligomer substrate at variable (A) Co and Mn loadings ([Co]=[Mn]), (B) NaBr loadings, (C) temperatures, and (D) reaction times. Standard conditions for optimization utilize x = 0.003 mmol, y = 0.003 mmol, z = 2 h, T = 120 °C for 20 mg of acetyl oligomer substrate. For the standard conditions, oxidation yields are an average of four runs. Values from all other conditions are from single runs. Numerical data for this figure and individual compound yields for each bar are provided in Tables S7–S10 (products quantified by GC-FID and LC-MS).