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. Author manuscript; available in PMC: 2024 Jan 11.
Published in final edited form as: ACS Infect Dis. 2019 Jul 2;5(8):1456–1470. doi: 10.1021/acsinfecdis.9b00156

Table 2.

13C NMR data for compounds 51–54 in DMSO-d6 (100 MHz, δ in ppm)

δ C
Position 51 52 53 54

1 195.9 196.5 199.0 199.0
2 49.0 49.6 49.2 49.5
3 49.2 48.6 48.5 48.1
4 131.3 131.9 131.4 131.6
5 126.4 126.1 126.0 125.7
6 39.1 39.2 38.7 38.7
7 42.4 42.5 42.1 42.2
8 33.3 33.4 33.0 33.0
9 35.8 35.9 35.5 35.5
10 28.1 28.1 27.6 27.7
11 39.4 39.9 39.3 39.3
12 14.0 14.2 13.4 13.5
13 130.9 131.4 130.5 130.6
14 132.7 133.0 132.1 132.5
15 131.8 132.0 131.1 131.6
16 130.9 130.5 128.0 127.7
17 42.7 42.8 17.8 17.9
18 66.3 66.3
19 23.5 23.5
20 22.6 22.7 22.2 22.3
21 22.8 22.9 22.5 22.5
2’ 176.6 175.8 179.2 179.0
3’ 100.9 101.6 99.4 99.8
4’ 190.9 190.5 190.7 190.6
5’ 68.1 67.4 63.2 62.9
6’ 58.4 58.6 60.8 60.7
N-Me 27.2 27.3