Table 5. Experimental Conditions and Resulting Isomeric Ratios (Evaluated by Subsequent 1H NMR Spectra) Related to [2]CF3SO3.
| solvent, time, temperature | cis/trans ratio |
|---|---|
| EtOH, 4 h, reflux | 6 |
| EtOH, 7 h, reflux | 8 |
| acetone, 2.5 h, reflux | 18 |
| DMF, 4 h, 110°C | 9 |
| DMF, overnight, 110°C | 17 |