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. 2024 Jan 3;63(2):1054–1067. doi: 10.1021/acs.inorgchem.3c03408

Table 5. Experimental Conditions and Resulting Isomeric Ratios (Evaluated by Subsequent 1H NMR Spectra) Related to [2]CF3SO3.

solvent, time, temperature cis/trans ratio
EtOH, 4 h, reflux 6
EtOH, 7 h, reflux 8
acetone, 2.5 h, reflux 18
DMF, 4 h, 110°C 9
DMF, overnight, 110°C 17