Table 3.
Trueness as % recovery and precision as % RSD of repeatability (within-laboratory reproducibility) of target pesticides in tomato matrix spiked at 5, 10, and 40 µg/kg.
S. N. | Pesticide | Trueness | Precision as repeatability (within-laboratory reproducibility) | ||||
---|---|---|---|---|---|---|---|
5 (µg/kg) (n = 6) | 10 (µg/kg) (n = 6) | 40 (µg/kg) (n = 6) | 5 (µg/kg) | 10 (µg/kg) | 40 (µg/kg) | ||
% recovery | % RSD | ||||||
1 | 3-Hydroxycarbofuran | 93 | 94 | 86 | 4.7 (8.2) | 3.2 (4.8) | 2.3 (1.7) |
2 | Acephate | 81 | 80 | 81 | 2.4 (8.5) | 2.2 (6.4) | 1.0 (2.8) |
3 | Alachlor | 89 | 90 | 87 | 3.5 (14.5) | 3.6 (5.0) | 1.2 (1.6) |
4 | Aldicarb sulfone | 89 | 90 | 87 | 3.8 (8.3) | 3.3 (4.9) | 1.7 (1.6) |
5 | Aldicarb sulfoxide | 87 | 88 | 83 | 3.6 (5.9) | 3.5 (3.5) | 1.4 (1.5) |
6 | Aldicarb | 87 | 83 | 83 | 2.0 (8.7) | 2.2 (6.5) | 1.2 (2.2) |
7 | Carbaryl | ∗ | 77 | 83 | ∗ | 6.1 (11.7) | 5.0 (3.7) |
8 | Carbendazim | 91 | 86 | 92 | 3.1 (9.9) | 2.1 (8.3) | 1.1 (2.0) |
9 | Carbofuran | 87 | 85 | 79 | 2.5 (12.6) | 2.8 (7.5) | 2.4 (3.7) |
10 | Cyprodinil | 90 | 85 | 83 | 5.6 (5.5) | 3.9 (4.0) | 1.1 (1.6) |
11 | Dimethoate | 90 | 88 | 88 | 4.5 (7.0) | 2.3 (4.8) | 0.9 (1.3) |
12 | Ethoprophos | 91 | 90 | 90 | 2.4 (7.4) | 3.0 (4.1) | 1.0 (1.2) |
13 | Imazalil | 90 | 82 | 78 | 4.3 (13.3) | 4.3 (8.6) | 2.9 (4.6) |
14 | Imidacloprid | 104 | 120 | 110 | 5.0 (6.9) | 4.9 (4.1) | 1.3 (4.6) |
15 | Kresoxim-methyl | 90 | 90 | 86 | 2.5 (6.2) | 3.4 (2.8) | 1.0 (1.8) |
16 | Metalaxyl | 91 | 90 | 89 | 2.9 (5.6) | 2.4 (3.2) | 1.2 (1.1) |
17 | Methidathion | 90 | 93 | 88 | 3.2 (6.8) | 4.8 (3.6) | 1.8 (1.8) |
18 | Methiocarb | 91 | 93 | 86 | 2.1 (4.7) | 3.5 (3.1) | 1.4 (1.6) |
19 | Methomyl | 90 | 92 | 87 | 5.3 (6.7) | 4.0 (4.7) | 1.2 (1.9) |
20 | Monocrotophos | 87 | 90 | 88 | 2.9 (6.8) | 2.9 (3.2) | 1.2 (1.1) |
21 | Oxamyl | 89 | 93 | 86 | 3.9 (7.0) | 3.7 (3.2) | 1.7 (1.5) |
22 | Penconazole | 88 | 87 | 87 | 3.0 (6.4) | 3.2 (4.2) | 0.7 (1.4) |
23 | Propargite | 87 | 83 | 86 | 3.1 (5.4) | 2.5 (4.5) | 1.4 (2.0) |
24 | Propoxur | 90 | 90 | 84 | 1.9 (4.7) | 2.1 (1.8) | 1.1 (1.3) |
25 | Thiabendazole | 93 | 88 | 88 | 2.4 (6.5) | 2.9 (5.1) | 1.4 (1.3) |
26 | Trichlorfon | 106 | 117 | 113 | 3.4 (8.2) | 4.1 (4.5) | 0.8 (3.4) |
∗ For carbaryl, a recovery experiment was performed at the 10 µg/kg level.