Table 1. Systematic Parameter Variation of the Organosolv Treatments Performed in the Current Work.
treatment code (ethanol/water/acetone)] | time [min] | temperature [°C] | ethanol/water/acetone [% v/v/v] | catalyst (sulfuric acid) [mm] |
---|---|---|---|---|
A0-1(40/60/0) | 60 | 180 | 40/60/0 | 0 |
A0-2(30/60/10) | 60 | 180 | 30/60/10 | 0 |
A0-3(20/60/20) | 60 | 180 | 20/60/20 | 0 |
A0-4(50/50/0) | 60 | 180 | 50/50/0 | 0 |
A0-5(40/50/10) | 60 | 180 | 40/50/10 | 0 |
A0-6(30/50/20) | 60 | 180 | 30/50/20 | 0 |
A0-7(60/40/0) | 60 | 180 | 60/40/0 | 0 |
A0-8(45/40/15) | 60 | 180 | 45/40/15 | 0 |
A0-9(30/40/30) | 60 | 180 | 30/40/30 | 0 |
A0-10(70/30/0) | 60 | 180 | 70/30/0 | 0 |
A0-11(55/30/15) | 60 | 180 | 55/30/15 | 0 |
A0-12(40/30/30) | 60 | 180 | 40/30/30 | 0 |
A20-1(40/60/0) | 60 | 180 | 40/60/0 | 20 |
A20-2(30/60/10) | 60 | 180 | 30/60/10 | 20 |
A20-3(20/60/20) | 60 | 180 | 20/60/20 | 20 |
A20-4(50/50/0) | 60 | 180 | 50/50/0 | 20 |
A20-5(40/50/10) | 60 | 180 | 40/50/10 | 20 |
A20-6(30/50/20) | 60 | 180 | 30/50/20 | 20 |
A20-7(60/40/0) | 60 | 180 | 60/40/0 | 20 |
A20-8(45/40/15) | 60 | 180 | 45/40/15 | 20 |
A20-9(30/40/30) | 60 | 180 | 30/40/30 | 20 |
A20-10(70/30/0) | 60 | 180 | 70/30/0 | 20 |
A20-11(55/30/15) | 60 | 180 | 55/30/15 | 20 |
A20-12(40/30/30) | 60 | 180 | 40/30/30 | 20 |
N.B: The treatment labels are described by their acid content (A0 or A20 for 0 or 20 mm H2SO4, respectively), and the treatment number.