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. 2024 Jan 12;12(4):1666–1680. doi: 10.1021/acssuschemeng.3c07236

Table 1. Systematic Parameter Variation of the Organosolv Treatments Performed in the Current Work.

treatment code (ethanol/water/acetone)] time [min] temperature [°C] ethanol/water/acetone [% v/v/v] catalyst (sulfuric acid) [mm]
A0-1(40/60/0) 60 180 40/60/0 0
A0-2(30/60/10) 60 180 30/60/10 0
A0-3(20/60/20) 60 180 20/60/20 0
A0-4(50/50/0) 60 180 50/50/0 0
A0-5(40/50/10) 60 180 40/50/10 0
A0-6(30/50/20) 60 180 30/50/20 0
A0-7(60/40/0) 60 180 60/40/0 0
A0-8(45/40/15) 60 180 45/40/15 0
A0-9(30/40/30) 60 180 30/40/30 0
A0-10(70/30/0) 60 180 70/30/0 0
A0-11(55/30/15) 60 180 55/30/15 0
A0-12(40/30/30) 60 180 40/30/30 0
A20-1(40/60/0) 60 180 40/60/0 20
A20-2(30/60/10) 60 180 30/60/10 20
A20-3(20/60/20) 60 180 20/60/20 20
A20-4(50/50/0) 60 180 50/50/0 20
A20-5(40/50/10) 60 180 40/50/10 20
A20-6(30/50/20) 60 180 30/50/20 20
A20-7(60/40/0) 60 180 60/40/0 20
A20-8(45/40/15) 60 180 45/40/15 20
A20-9(30/40/30) 60 180 30/40/30 20
A20-10(70/30/0) 60 180 70/30/0 20
A20-11(55/30/15) 60 180 55/30/15 20
A20-12(40/30/30) 60 180 40/30/30 20

N.B: The treatment labels are described by their acid content (A0 or A20 for 0 or 20 mm H2SO4, respectively), and the treatment number.