Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Li2(C12H8O6S2)(H2O)2] |
| M r | 362.22 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 286 |
| a, b, c (Å) | 15.8584 (11), 5.3693 (4), 8.8636 (6) |
| β (°) | 99.994 (7) |
| V (Å3) | 743.27 (9) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.40 |
| Crystal size (mm) | 0.50 × 0.40 × 0.20 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS RAPID |
| Absorption correction | Multi-scan (ABSCOR; Rigaku, 1995 ▸) |
| T min, T max | 0.213, 0.924 |
| No. of measured, independent and observed [F 2 > 2.0σ(F 2)] reflections | 9858, 1666, 1490 |
| R int | 0.067 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.061, 0.159, 1.12 |
| No. of reflections | 1666 |
| No. of parameters | 133 |
| No. of restraints | 3 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.74, −0.28 |