Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Li(C6H6N)(C4H8O)3] |
| M r | 315.37 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 9.267 (3), 13.178 (4), 15.053 (5) |
| β (°) | 94.437 (6) |
| V (Å3) | 1832.7 (10) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.08 |
| Crystal size (mm) | 0.39 × 0.29 × 0.21 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.493, 0.570 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 58129, 10326, 7724 |
| R int | 0.048 |
| (sin θ/λ)max (Å−1) | 0.909 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.052, 0.159, 1.04 |
| No. of reflections | 10326 |
| No. of parameters | 226 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.68, −0.39 |