| Crystal data |
| Chemical formula |
C24H29F2NO4
|
|
M
r
|
433.48 |
| Crystal system, space group |
Orthorhombic, P
c
a21
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
11.9879 (7), 12.1807 (7), 15.4518 (9) |
|
V (Å3) |
2256.3 (2) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.10 |
| Crystal size (mm) |
0.27 × 0.24 × 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker Quest D8 with Photon 2 detector |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.718, 0.744 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
103269, 9491, 7264 |
|
R
int
|
0.080 |
| (sin θ/λ)max (Å−1) |
0.826 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.107, 1.03 |
| No. of reflections |
9491 |
| No. of parameters |
289 |
| No. of restraints |
1 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.32, −0.29 |
| Absolute structure |
Flack x determined using 2721 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.0 (2) |
