Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Bi2O2(OH)](NO3) |
| M r | 528.98 |
| Crystal system, space group | Orthorhombic, P n a21 |
| Temperature (K) | 100 |
| a, b, c (Å) | 5.3854 (13), 5.3676 (13), 17.051 (4) |
| V (Å3) | 492.9 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 71.27 |
| Crystal size (mm) | 0.09 × 0.08 × 0.01 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Numerical (HABITUS; Herrendorf, 1997 ▸) |
| T min, T max | 0.017, 0.524 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 9853, 2798, 2407 |
| R int | 0.062 |
| (sin θ/λ)max (Å−1) | 0.881 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.030, 0.057, 0.98 |
| No. of reflections | 2798 |
| No. of parameters | 48 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters not defined |
| Δρmax, Δρmin (e Å−3) | 3.13, −3.61 |
| Absolute structure | Twinning involves inversion, so Flack parameter cannot be determined |