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(a) Temperature data for OCT–FDM of a 5% sucrose solution, 0.6 mL. (b) Temperature data for OCT–FDM of a 5% sucrose solution, 1.25 mL. (c) Temperature data for OCT–FDM of a 5% sucrose solution, 1.25 mL slow ramp rate. (d) Temperature data for OCT–FDM of a 5% sucrose solution, 1.25 mL TC on side of the vial. ST, shelf temperature; CT, commanded temperature; Tp, product temperature; Tp1, product temperature 1; Tp2, product temperature 2; and Ts, temperature side of vial.
