FIGURE 10.
Novel in situ combined small‐angle X‐ray scattering/X‐ray diffraction/X‐ray absorption fine structure technique. (A) Schematic map of the SAXS/XRD/XAFS combined setup. (B) Photo of the SAXS/XRD/XAFS combined setup equipped in beamline 1W2B of BSRF. (C) SAXS (left panel) and XRD (middle panel) patterns as well as XAFS (right panel) spectra acquired by the SAXS/XRD/XAFS combined technique in two‐way energy‐scanning strategy with high‐frequency sampling scheme (100 kHz) for the Cu powder. (D) SAXS (left panel) and XRD (middle panel) patterns as well as XAFS (right panel) spectra acquired by in situ SAXS/XRD/XAFS combined technique in traditional one‐way energy‐scanning strategy for the hydrothermal synthesis of (BiO)2CO3 particles at temperature of 423 K and pressure of 3 MPa. Reproduced with permission.[ 137 ] Copyright 2023, Springer.