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. 2024 Feb 19;14(9):5941–5958. doi: 10.1039/d4ra00290c

Table 1. Independent factors used for CCD in the transesterification of enriched glycerol and DMC with the 5%Li/MCM-41 solid catalyst (response variable is the GC yield).

Factor Unit Symbols Coded factor levels
−2 −1 0 +1 +2
Catalyst loading wt% relative to the initial amount of enriched glycerol A 2 3 4 5 6
DMC: enriched glycerol molar ratio B 1 : 1 2 : 1 3 : 1 4 : 1 5 : 1
Reaction temperature °C C 70 75 80 85 90
Reaction time min D 60 90 120 150 180