Table 1. Independent factors used for CCD in the transesterification of enriched glycerol and DMC with the 5%Li/MCM-41 solid catalyst (response variable is the GC yield).
| Factor | Unit | Symbols | Coded factor levels | ||||
|---|---|---|---|---|---|---|---|
| −2 | −1 | 0 | +1 | +2 | |||
| Catalyst loading | wt% relative to the initial amount of enriched glycerol | A | 2 | 3 | 4 | 5 | 6 |
| DMC: enriched glycerol molar ratio | — | B | 1 : 1 | 2 : 1 | 3 : 1 | 4 : 1 | 5 : 1 |
| Reaction temperature | °C | C | 70 | 75 | 80 | 85 | 90 |
| Reaction time | min | D | 60 | 90 | 120 | 150 | 180 |