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Validation of LC-MS/MS for the detection of the algal toxins analyzed.
| Concentration Level (µg/Kg) | Repeatability (µg/Kg) | LOD (µg/Kg) | LOQ (µg/Kg) | Mean Recovery (%) |
|---|---|---|---|---|
| OA | ||||
| 40 | 7.6 | 21.6 | 26.4 | 77 |
| 160 | 14.6 | |||
| DTX1 | ||||
| 40 | 5.1 | 23.3 | 28.3 | 114 |
| 160 | 19.1 | |||
| DTX2 | ||||
| 40 | 18.9 | 24 | 27 | 96 |
| 160 | 12.3 | |||
| AZA1 | ||||
| 40 | 6 | 9.1 | 10.6 | 60 |
| 160 | 16.4 | |||
| AZA3 | ||||
| 40 | 4.3 | 6.5 | 8.1 | 70 |
| 160 | 11.2 | |||
| PTX2 | ||||
| 40 | 7.5 | 18.4 | 26.2 | 63 |
| 160 | 13 | |||
| YTX | ||||
| 100 | 11.7 | 55 | 61.2 | 78 |
| 400 | 45.3 | |||
