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. 2023 Dec 4;6(1):102–114. doi: 10.1007/s42995-023-00210-0

Table 2.

13C NMR data of 1 − 4 in CDCl3

No 1a 2a 3b 4b
2 92.3, C 88.1, C 93.0, C 89.4, C
3 190.8, C 194.6, C 190.8, C 194.2, C
3a 104.1, C 105.3, C 105.0, C 105.9, C
4 159.6, C 159.3, C 158.3, C 158.0, C
5 93.9, CH 93.9, CH 90.1, CH 89.9, CH
6 170.7, C 171.0, C 165.0, C 165.2, C
7 89.0, CH 89.1, CH 97.8, C 97.9, C
7a 175.9, C 175.9, C 169.3, C 169.3, C
2' 168.7, C 169.1, C 168.1, C 168.5, C
3' 104.0, CH 104.9, CH 104.2, CH 105.1, CH
4' 195.7, C 195.9, C 195.4, C 195.6, C
5' 46.1, CH2 47.2, CH2 46.1, CH2 47.2, CH2
6' 74.8, C 74.5, C 74.7, C 74.7, C
4-OCH3 56.3, CH3 56.4, CH3 56.6, CH3 56.6, CH3
6-OCH3 56.3, CH3 56.4, CH3 57.2, CH3 57.2, CH3
2'-OCH3 56.8, CH3 56.8, CH3 56.9, CH3 56.9, CH3
6'-CH3 23.3, CH3 23.7, CH3 23.3, CH3 23.9, CH3

a13C NMR tested with 100 MHz.

b13C NMR tested with 150 MHz.