| Crystal data |
| Chemical formula |
[Zn2(C2H3O2)4(C11H9N3O)2] |
|
M
r
|
765.34 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.3549 (7), 9.3366 (8), 12.3971 (7) |
| α, β, γ (°) |
69.409 (7), 75.524 (6), 65.217 (8) |
|
V (Å3) |
815.88 (13) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.54 |
| Crystal size (mm) |
0.35 × 0.32 × 0.31 |
| |
| Data collection |
| Diffractometer |
Xcalibur, Sapphire3 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2019 ▸) |
|
Tmin, Tmax
|
0.907, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
10420, 5737, 4546 |
|
R
int
|
0.022 |
| (sin θ/λ)max (Å−1) |
0.778 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.039, 0.098, 1.03 |
| No. of reflections |
5737 |
| No. of parameters |
223 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.66, −0.22 |
