| Crystal data |
| Chemical formula |
C30H25NO |
|
M
r
|
415.51 |
| Crystal system, space group |
Orthorhombic, Fdd2 |
| Temperature (K) |
150 |
|
a, b, c (Å) |
27.8745 (9), 83.475 (3), 7.5368 (2) |
|
V (Å3) |
17536.7 (10) |
|
Z
|
32 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.58 |
| Crystal size (mm) |
0.33 × 0.13 × 0.06 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
Tmin, Tmax
|
0.833, 0.968 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
48787, 7883, 7093 |
|
R
int
|
0.039 |
| (sin θ/λ)max (Å−1) |
0.618 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.032, 0.088, 1.05 |
| No. of reflections |
7883 |
| No. of parameters |
583 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.14, −0.12 |
| Absolute structure |
Flack x determined using 2576 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.05 (11) |
