| Crystal data |
| Chemical formula |
[Pd(C10H8N2)(C12H12N2O2)](CF3SO3)2
|
|
M
r
|
776.96 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
14.4340 (3), 13.9644 (2), 14.2126 (2) |
| β (°) |
102.5361 (16) |
|
V (Å3) |
2796.41 (8) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
7.64 |
| Crystal size (mm) |
0.23 × 0.11 × 0.08 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2022 ▸) |
|
Tmin, Tmax
|
0.512, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
26480, 5585, 5101 |
|
R
int
|
0.053 |
| (sin θ/λ)max (Å−1) |
0.630 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.038, 0.100, 1.04 |
| No. of reflections |
5585 |
| No. of parameters |
408 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.80, −1.09 |
