| Crystal data |
| Chemical formula |
[Ru(C10H8N2)2(C6H6N2O(H2O)](CF3SO3)2
|
|
M
r
|
851.72 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
9.7878 (1), 26.2103 (3), 12.6443 (1) |
| β (°) |
97.202 (1) |
|
V (Å3) |
3218.19 (6) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
6.02 |
| Crystal size (mm) |
0.11 × 0.06 × 0.04 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2023 ▸) |
|
Tmin, Tmax
|
0.099, 0.513 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
35289, 5777, 5536 |
|
R
int
|
0.072 |
| (sin θ/λ)max (Å−1) |
0.599 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.071, 0.159, 1.06 |
| No. of reflections |
5777 |
| No. of parameters |
496 |
| No. of restraints |
25 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.34, −1.09 |
