Si1—O1 | 1.7910 (9) | C14—F3 | 1.3353 (15) |
Si1—O4 | 1.8042 (9) | C14—C15 | 1.3814 (19) |
Si1—O3 | 1.8480 (9) | C15—F4 | 1.3430 (14) |
Si1—O2 | 1.8503 (9) | C15—C16 | 1.3853 (17) |
Si1—C11 | 1.9559 (12) | C16—F5 | 1.3557 (14) |
Si1—C17 | 1.9683 (12) | C17—C18 | 1.3904 (18) |
O1—C1' | 1.3324 (14) | C17—C22 | 1.3957 (17) |
O1—N1 | 1.3324 (14) | C18—F6 | 1.3543 (15) |
O2—N1' | 1.3244 (14) | C18—C19 | 1.3903 (18) |
O2—C1 | 1.3244 (14) | C19—F7 | 1.3431 (18) |
O3—C6' | 1.3263 (13) | C19—C20 | 1.377 (2) |
O3—N2 | 1.3263 (13) | C20—F8 | 1.3452 (17) |
O4—N2' | 1.3348 (13) | C20—C21 | 1.375 (2) |
O4—C6 | 1.3348 (13) | C21—F9 | 1.3462 (17) |
N1—C1 | 1.3562 (14) | C21—C22 | 1.3874 (18) |
N1—C5 | 1.3714 (16) | C22—F10 | 1.3513 (16) |
C1—C2 | 1.3686 (17) | C23—C24 | 1.434 (10) |
N2—C6 | 1.3487 (15) | C23—H23A | 0.9800 |
N2—C10 | 1.3706 (16) | C23—H23B | 0.9800 |
C6—C7 | 1.3740 (15) | C23—H23C | 0.9800 |
N1'—C1' | 1.3562 (14) | C24—C25 | 1.553 (8) |
N1'—C2 | 1.3686 (17) | C24—H24A | 0.9900 |
C1'—C5 | 1.3714 (16) | C24—H24B | 0.9900 |
N2'—C6' | 1.3487 (15) | C25—C26 | 1.552 (10) |
N2'—C7 | 1.3740 (15) | C25—H25A | 0.9900 |
C6'—C10 | 1.3706 (16) | C25—H25B | 0.9900 |
C2—C3 | 1.3732 (19) | C26—C27 | 1.491 (10) |
C2—H2 | 0.9500 | C26—H26A | 0.9900 |
C3—C4 | 1.4013 (19) | C26—H26B | 0.9900 |
C3—H3 | 0.9500 | C27—H27A | 0.9800 |
C4—C5 | 1.3828 (19) | C27—H27B | 0.9800 |
C4—H4 | 0.9500 | C27—H27C | 0.9800 |
C5—H5 | 0.9500 | O5'—C23' | 1.432 (5) |
C7—C8 | 1.3770 (18) | O5'—C26' | 1.456 (10) |
C7—H7 | 0.9500 | C23'—C24' | 1.498 (6) |
C8—C9 | 1.398 (2) | C23'—H23D | 0.9900 |
C8—H8 | 0.9500 | C23'—H23E | 0.9900 |
C9—C10 | 1.3776 (19) | C24'—C25' | 1.482 (8) |
C9—H9 | 0.9500 | C24'—H24C | 0.9900 |
C10—H10 | 0.9500 | C24'—H24D | 0.9900 |
C11—C16 | 1.3923 (16) | C25'—C26' | 1.494 (11) |
C11—C12 | 1.3937 (16) | C25'—H25C | 0.9900 |
C12—F1 | 1.3545 (14) | C25'—H25D | 0.9900 |
C12—C13 | 1.3851 (17) | C26'—H26C | 0.9900 |
C13—F2 | 1.3428 (14) | C26'—H26D | 0.9900 |
C13—C14 | 1.3861 (19) | ||
O1—Si1—O4 | 166.74 (4) | C12—C13—C14 | 119.49 (11) |
O1—Si1—O3 | 86.65 (4) | F3—C14—C15 | 120.33 (12) |
O4—Si1—O3 | 84.60 (4) | F3—C14—C13 | 120.99 (12) |
O1—Si1—O2 | 85.17 (4) | C15—C14—C13 | 118.65 (11) |
O4—Si1—O2 | 84.53 (4) | F4—C15—C14 | 119.78 (11) |
O3—Si1—O2 | 87.56 (4) | F4—C15—C16 | 120.51 (11) |
O1—Si1—C11 | 91.41 (4) | C14—C15—C16 | 119.71 (11) |
O4—Si1—C11 | 98.54 (4) | F5—C16—C15 | 115.00 (10) |
O3—Si1—C11 | 90.16 (4) | F5—C16—C11 | 120.69 (10) |
O2—Si1—C11 | 175.99 (5) | C15—C16—C11 | 124.29 (11) |
O1—Si1—C17 | 99.44 (5) | C18—C17—C22 | 113.39 (11) |
O4—Si1—C17 | 88.68 (4) | C18—C17—Si1 | 122.91 (9) |
O3—Si1—C17 | 172.66 (4) | C22—C17—Si1 | 123.45 (9) |
O2—Si1—C17 | 88.88 (5) | F6—C18—C19 | 115.25 (12) |
C11—Si1—C17 | 93.75 (5) | F6—C18—C17 | 120.49 (11) |
C1'—O1—Si1 | 112.84 (7) | C19—C18—C17 | 124.25 (12) |
N1—O1—Si1 | 112.84 (7) | F7—C19—C20 | 119.76 (13) |
N1'—O2—Si1 | 111.23 (7) | F7—C19—C18 | 120.96 (14) |
C1—O2—Si1 | 111.23 (7) | C20—C19—C18 | 119.28 (13) |
C6'—O3—Si1 | 110.81 (7) | F8—C20—C21 | 120.52 (15) |
N2—O3—Si1 | 110.81 (7) | F8—C20—C19 | 120.04 (15) |
N2'—O4—Si1 | 111.71 (7) | C21—C20—C19 | 119.44 (13) |
C6—O4—Si1 | 111.71 (7) | F9—C21—C20 | 119.99 (13) |
O1—N1—C1 | 114.69 (9) | F9—C21—C22 | 120.74 (14) |
O1—N1—C5 | 124.26 (10) | C20—C21—C22 | 119.27 (13) |
C1—N1—C5 | 121.02 (11) | F10—C22—C21 | 114.91 (11) |
O2—C1—N1 | 114.61 (10) | F10—C22—C17 | 120.77 (10) |
O2—C1—C2 | 123.66 (10) | C21—C22—C17 | 124.32 (13) |
N1—C1—C2 | 121.70 (10) | C24—C23—H23A | 109.5 |
O3—N2—C6 | 114.78 (9) | C24—C23—H23B | 109.5 |
O3—N2—C10 | 124.02 (10) | H23A—C23—H23B | 109.5 |
C6—N2—C10 | 121.20 (10) | C24—C23—H23C | 109.5 |
O4—C6—N2 | 114.45 (9) | H23A—C23—H23C | 109.5 |
O4—C6—C7 | 124.04 (10) | H23B—C23—H23C | 109.5 |
N2—C6—C7 | 121.50 (10) | C23—C24—C25 | 115.3 (6) |
O2—N1'—C1' | 114.61 (10) | C23—C24—H24A | 108.4 |
O2—N1'—C2 | 123.66 (10) | C25—C24—H24A | 108.4 |
C1'—N1'—C2 | 121.70 (10) | C23—C24—H24B | 108.4 |
O1—C1'—N1' | 114.69 (9) | C25—C24—H24B | 108.4 |
O1—C1'—C5 | 124.26 (10) | H24A—C24—H24B | 107.5 |
N1'—C1'—C5 | 121.02 (11) | C26—C25—C24 | 109.8 (6) |
O4—N2'—C6' | 114.45 (9) | C26—C25—H25A | 109.7 |
O4—N2'—C7 | 124.04 (10) | C24—C25—H25A | 109.7 |
C6'—N2'—C7 | 121.50 (10) | C26—C25—H25B | 109.7 |
O3—C6'—N2' | 114.78 (9) | C24—C25—H25B | 109.7 |
O3—C6'—C10 | 124.02 (10) | H25A—C25—H25B | 108.2 |
N2'—C6'—C10 | 121.20 (10) | C27—C26—C25 | 114.5 (6) |
N1'—C2—C3 | 118.72 (11) | C27—C26—H26A | 108.6 |
C1—C2—C3 | 118.72 (11) | C25—C26—H26A | 108.6 |
C1—C2—H2 | 120.6 | C27—C26—H26B | 108.6 |
C3—C2—H2 | 120.6 | C25—C26—H26B | 108.6 |
C2—C3—C4 | 119.88 (12) | H26A—C26—H26B | 107.6 |
C2—C3—H3 | 120.1 | C26—C27—H27A | 109.5 |
C4—C3—H3 | 120.1 | C26—C27—H27B | 109.5 |
C5—C4—C3 | 120.26 (12) | H27A—C27—H27B | 109.5 |
C5—C4—H4 | 119.9 | C26—C27—H27C | 109.5 |
C3—C4—H4 | 119.9 | H27A—C27—H27C | 109.5 |
C1'—C5—C4 | 118.42 (11) | H27B—C27—H27C | 109.5 |
N1—C5—C4 | 118.42 (11) | C23'—O5'—C26' | 109.5 (5) |
N1—C5—H5 | 120.8 | O5'—C23'—C24' | 104.9 (4) |
C4—C5—H5 | 120.8 | O5'—C23'—H23D | 110.8 |
N2'—C7—C8 | 118.54 (11) | C24'—C23'—H23D | 110.8 |
C6—C7—C8 | 118.54 (11) | O5'—C23'—H23E | 110.8 |
C6—C7—H7 | 120.7 | C24'—C23'—H23E | 110.8 |
C8—C7—H7 | 120.7 | H23D—C23'—H23E | 108.8 |
C7—C8—C9 | 119.84 (11) | C25'—C24'—C23' | 102.3 (4) |
C7—C8—H8 | 120.1 | C25'—C24'—H24C | 111.3 |
C9—C8—H8 | 120.1 | C23'—C24'—H24C | 111.3 |
C10—C9—C8 | 120.24 (12) | C25'—C24'—H24D | 111.3 |
C10—C9—H9 | 119.9 | C23'—C24'—H24D | 111.3 |
C8—C9—H9 | 119.9 | H24C—C24'—H24D | 109.2 |
C6'—C10—C9 | 118.59 (12) | C24'—C25'—C26' | 105.0 (6) |
N2—C10—C9 | 118.59 (12) | C24'—C25'—H25C | 110.7 |
N2—C10—H10 | 120.7 | C26'—C25'—H25C | 110.7 |
C9—C10—H10 | 120.7 | C24'—C25'—H25D | 110.7 |
C16—C11—C12 | 113.42 (10) | C26'—C25'—H25D | 110.7 |
C16—C11—Si1 | 123.97 (8) | H25C—C25'—H25D | 108.8 |
C12—C11—Si1 | 122.43 (8) | O5'—C26'—C25' | 104.9 (7) |
F1—C12—C13 | 115.50 (10) | O5'—C26'—H26C | 110.8 |
F1—C12—C11 | 120.11 (10) | C25'—C26'—H26C | 110.8 |
C13—C12—C11 | 124.37 (11) | O5'—C26'—H26D | 110.8 |
F2—C13—C12 | 120.66 (12) | C25'—C26'—H26D | 110.8 |
F2—C13—C14 | 119.84 (11) | H26C—C26'—H26D | 108.8 |
O4—Si1—O1—C1' | −28.5 (2) | O1—C1'—C5—C4 | 178.47 (11) |
O3—Si1—O1—C1' | −77.23 (8) | N1'—C1'—C5—C4 | 0.59 (18) |
O2—Si1—O1—C1' | 10.60 (8) | O1—N1—C5—C4 | 178.47 (11) |
C11—Si1—O1—C1' | −167.31 (8) | C1—N1—C5—C4 | 0.59 (18) |
C17—Si1—O1—C1' | 98.65 (8) | C3—C4—C5—C1' | −0.66 (19) |
O4—Si1—O1—N1 | −28.5 (2) | C3—C4—C5—N1 | −0.66 (19) |
O3—Si1—O1—N1 | −77.23 (8) | O4—N2'—C7—C8 | 176.47 (11) |
O2—Si1—O1—N1 | 10.60 (8) | C6'—N2'—C7—C8 | −3.09 (18) |
C11—Si1—O1—N1 | −167.31 (8) | O4—C6—C7—C8 | 176.47 (11) |
C17—Si1—O1—N1 | 98.65 (8) | N2—C6—C7—C8 | −3.09 (18) |
O1—Si1—O2—N1' | −10.44 (7) | N2'—C7—C8—C9 | 0.8 (2) |
O4—Si1—O2—N1' | 161.20 (8) | C6—C7—C8—C9 | 0.8 (2) |
O3—Si1—O2—N1' | 76.40 (7) | C7—C8—C9—C10 | 1.3 (2) |
C17—Si1—O2—N1' | −110.02 (8) | O3—C6'—C10—C9 | 179.41 (13) |
O1—Si1—O2—C1 | −10.44 (7) | N2'—C6'—C10—C9 | −1.0 (2) |
O4—Si1—O2—C1 | 161.20 (8) | O3—N2—C10—C9 | 179.41 (13) |
O3—Si1—O2—C1 | 76.40 (7) | C6—N2—C10—C9 | −1.0 (2) |
C17—Si1—O2—C1 | −110.02 (8) | C8—C9—C10—C6' | −1.3 (2) |
O1—Si1—O3—C6' | 154.54 (8) | C8—C9—C10—N2 | −1.3 (2) |
O4—Si1—O3—C6' | −15.49 (8) | C16—C11—C12—F1 | 179.86 (10) |
O2—Si1—O3—C6' | 69.23 (8) | Si1—C11—C12—F1 | 4.45 (15) |
C11—Si1—O3—C6' | −114.06 (8) | C16—C11—C12—C13 | 1.43 (17) |
O1—Si1—O3—N2 | 154.54 (8) | Si1—C11—C12—C13 | −173.97 (9) |
O4—Si1—O3—N2 | −15.49 (8) | F1—C12—C13—F2 | 1.51 (17) |
O2—Si1—O3—N2 | 69.23 (8) | C11—C12—C13—F2 | 180.00 (11) |
C11—Si1—O3—N2 | −114.06 (8) | F1—C12—C13—C14 | −177.48 (11) |
O1—Si1—O4—N2' | −31.6 (2) | C11—C12—C13—C14 | 1.01 (19) |
O3—Si1—O4—N2' | 17.32 (7) | F2—C13—C14—F3 | −3.34 (18) |
O2—Si1—O4—N2' | −70.74 (8) | C12—C13—C14—F3 | 175.65 (11) |
C11—Si1—O4—N2' | 106.66 (8) | F2—C13—C14—C15 | 178.54 (11) |
C17—Si1—O4—N2' | −159.74 (8) | C12—C13—C14—C15 | −2.46 (18) |
O1—Si1—O4—C6 | −31.6 (2) | F3—C14—C15—F4 | 2.55 (18) |
O3—Si1—O4—C6 | 17.32 (7) | C13—C14—C15—F4 | −179.32 (11) |
O2—Si1—O4—C6 | −70.74 (8) | F3—C14—C15—C16 | −176.71 (11) |
C11—Si1—O4—C6 | 106.66 (8) | C13—C14—C15—C16 | 1.41 (18) |
C17—Si1—O4—C6 | −159.74 (8) | F4—C15—C16—F5 | 0.51 (16) |
Si1—O1—N1—C1 | −8.78 (12) | C14—C15—C16—F5 | 179.77 (11) |
Si1—O1—N1—C5 | 173.22 (9) | F4—C15—C16—C11 | −178.03 (11) |
Si1—O2—C1—N1 | 8.22 (12) | C14—C15—C16—C11 | 1.23 (19) |
Si1—O2—C1—C2 | −173.65 (9) | C12—C11—C16—F5 | 178.98 (10) |
O1—N1—C1—O2 | 0.12 (14) | Si1—C11—C16—F5 | −5.70 (16) |
C5—N1—C1—O2 | 178.19 (10) | C12—C11—C16—C15 | −2.56 (17) |
O1—N1—C1—C2 | −178.04 (10) | Si1—C11—C16—C15 | 172.76 (9) |
C5—N1—C1—C2 | 0.02 (17) | C22—C17—C18—F6 | 178.41 (11) |
Si1—O3—N2—C6 | 10.62 (12) | Si1—C17—C18—F6 | −7.13 (16) |
Si1—O3—N2—C10 | −169.72 (11) | C22—C17—C18—C19 | −2.95 (19) |
Si1—O4—C6—N2 | −15.96 (12) | Si1—C17—C18—C19 | 171.50 (11) |
Si1—O4—C6—C7 | 164.44 (9) | F6—C18—C19—F7 | 1.0 (2) |
O3—N2—C6—O4 | 3.27 (15) | C17—C18—C19—F7 | −177.71 (13) |
C10—N2—C6—O4 | −176.40 (11) | F6—C18—C19—C20 | −179.78 (14) |
O3—N2—C6—C7 | −177.13 (11) | C17—C18—C19—C20 | 1.5 (2) |
C10—N2—C6—C7 | 3.20 (18) | F7—C19—C20—F8 | −0.9 (3) |
Si1—O2—N1'—C1' | 8.22 (12) | C18—C19—C20—F8 | 179.89 (15) |
Si1—O2—N1'—C2 | −173.65 (9) | F7—C19—C20—C21 | 179.80 (15) |
Si1—O1—C1'—N1' | −8.78 (12) | C18—C19—C20—C21 | 0.6 (2) |
Si1—O1—C1'—C5 | 173.22 (9) | F8—C20—C21—F9 | 0.5 (3) |
O2—N1'—C1'—O1 | 0.12 (14) | C19—C20—C21—F9 | 179.87 (15) |
C2—N1'—C1'—O1 | −178.04 (10) | F8—C20—C21—C22 | 179.77 (15) |
O2—N1'—C1'—C5 | 178.19 (10) | C19—C20—C21—C22 | −0.9 (3) |
C2—N1'—C1'—C5 | 0.02 (17) | F9—C21—C22—F10 | −0.7 (2) |
Si1—O4—N2'—C6' | −15.96 (12) | C20—C21—C22—F10 | −179.93 (14) |
Si1—O4—N2'—C7 | 164.44 (9) | F9—C21—C22—C17 | 178.44 (13) |
Si1—O3—C6'—N2' | 10.62 (12) | C20—C21—C22—C17 | −0.8 (2) |
Si1—O3—C6'—C10 | −169.72 (11) | C18—C17—C22—F10 | −178.32 (11) |
O4—N2'—C6'—O3 | 3.27 (15) | Si1—C17—C22—F10 | 7.26 (17) |
C7—N2'—C6'—O3 | −177.13 (11) | C18—C17—C22—C21 | 2.58 (19) |
O4—N2'—C6'—C10 | −176.40 (11) | Si1—C17—C22—C21 | −171.84 (11) |
C7—N2'—C6'—C10 | 3.20 (18) | C23—C24—C25—C26 | −72.1 (8) |
O2—N1'—C2—C3 | −178.57 (11) | C24—C25—C26—C27 | 173.7 (6) |
C1'—N1'—C2—C3 | −0.58 (18) | C26'—O5'—C23'—C24' | −20.7 (6) |
O2—C1—C2—C3 | −178.57 (11) | O5'—C23'—C24'—C25' | 34.3 (6) |
N1—C1—C2—C3 | −0.58 (18) | C23'—C24'—C25'—C26' | −35.2 (7) |
N1'—C2—C3—C4 | 0.5 (2) | C23'—O5'—C26'—C25' | −1.3 (7) |
C1—C2—C3—C4 | 0.5 (2) | C24'—C25'—C26'—O5' | 23.2 (8) |
C2—C3—C4—C5 | 0.1 (2) |