| Crystal data |
| Chemical formula |
[Cu2(C13H17O3)4(C2H6OS)2] |
|
M
r
|
1168.40 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
180 |
|
a, b, c (Å) |
10.2990 (17), 11.734 (2), 12.846 (2) |
| α, β, γ (°) |
87.275 (3), 88.918 (3), 72.096 (2) |
|
V (Å3) |
1475.6 (4) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.85 |
| Crystal size (mm) |
0.13 × 0.08 × 0.05 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Empirical (using intensity measurements) (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.692, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
19892, 6767, 4879 |
|
R
int
|
0.046 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.047, 0.130, 1.09 |
| No. of reflections |
6767 |
| No. of parameters |
367 |
| No. of restraints |
12 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.61, −0.52 |
