O1—C5 | 1.236 (3) | C12—H12C | 0.9800 |
O2—C13 | 1.212 (3) | C14—H14A | 0.9800 |
O3—C13 | 1.358 (4) | C14—H14B | 0.9800 |
O3—C14 | 1.447 (4) | C14—H14C | 0.9800 |
N1—C1 | 1.363 (3) | C15—C16 | 1.3900 |
N1—C9 | 1.378 (3) | C15—C20 | 1.3900 |
N1—H1N | 0.90 (3) | C16—C17 | 1.3900 |
C1—C6 | 1.357 (3) | C16—H16A | 0.9500 |
C1—C2 | 1.499 (3) | C17—C18 | 1.3900 |
C2—C3 | 1.533 (4) | C17—H17A | 0.9500 |
C2—H2A | 0.9900 | C18—C19 | 1.3900 |
C2—H2B | 0.9900 | C18—O4 | 1.400 (3) |
C3—C4 | 1.524 (4) | C19—C20 | 1.3900 |
C3—C10 | 1.532 (4) | C19—H19A | 0.9500 |
C3—C11 | 1.535 (4) | C20—H20A | 0.9500 |
C4—C5 | 1.505 (3) | O4—C21 | 1.330 (6) |
C4—H4A | 0.9900 | C21—F2 | 1.375 (7) |
C4—H4B | 0.9900 | C21—F1 | 1.379 (8) |
C5—C6 | 1.436 (3) | C21—H21A | 1.0000 |
C6—C7 | 1.512 (3) | C15A—C16A | 1.3900 |
C7—C15 | 1.518 (3) | C15A—C20A | 1.3900 |
C7—C8 | 1.522 (3) | C16A—C17A | 1.3900 |
C7—C15A | 1.589 (4) | C16A—H16B | 0.9500 |
C7—H7 | 0.97 (3) | C17A—C18A | 1.3900 |
C8—C9 | 1.354 (4) | C17A—H17B | 0.9500 |
C8—C13 | 1.465 (4) | C18A—C19A | 1.3900 |
C9—C12 | 1.501 (4) | C18A—O4A | 1.399 (4) |
C10—H10A | 0.9800 | C19A—C20A | 1.3900 |
C10—H10B | 0.9800 | C19A—H19B | 0.9500 |
C10—H10C | 0.9800 | C20A—H20B | 0.9500 |
C11—H11A | 0.9800 | O4A—C21A | 1.334 (7) |
C11—H11B | 0.9800 | C21A—F2A | 1.370 (7) |
C11—H11C | 0.9800 | C21A—F1A | 1.379 (9) |
C12—H12A | 0.9800 | C21A—H21B | 1.0000 |
C12—H12B | 0.9800 | ||
C13—O3—C14 | 114.9 (3) | H12A—C12—H12C | 109.5 |
C1—N1—C9 | 123.2 (2) | H12B—C12—H12C | 109.5 |
C1—N1—H1N | 117 (2) | O2—C13—O3 | 121.4 (3) |
C9—N1—H1N | 119 (2) | O2—C13—C8 | 128.5 (3) |
C6—C1—N1 | 120.3 (2) | O3—C13—C8 | 110.0 (2) |
C6—C1—C2 | 122.7 (2) | O3—C14—H14A | 109.5 |
N1—C1—C2 | 116.9 (2) | O3—C14—H14B | 109.5 |
C1—C2—C3 | 112.34 (19) | H14A—C14—H14B | 109.5 |
C1—C2—H2A | 109.1 | O3—C14—H14C | 109.5 |
C3—C2—H2A | 109.1 | H14A—C14—H14C | 109.5 |
C1—C2—H2B | 109.1 | H14B—C14—H14C | 109.5 |
C3—C2—H2B | 109.1 | C16—C15—C20 | 120.0 |
H2A—C2—H2B | 107.9 | C16—C15—C7 | 119.0 (2) |
C4—C3—C10 | 110.0 (3) | C20—C15—C7 | 120.9 (2) |
C4—C3—C2 | 108.1 (2) | C15—C16—C17 | 120.0 |
C10—C3—C2 | 109.2 (2) | C15—C16—H16A | 120.0 |
C4—C3—C11 | 110.3 (2) | C17—C16—H16A | 120.0 |
C10—C3—C11 | 108.7 (2) | C16—C17—C18 | 120.0 |
C2—C3—C11 | 110.6 (3) | C16—C17—H17A | 120.0 |
C5—C4—C3 | 114.5 (2) | C18—C17—H17A | 120.0 |
C5—C4—H4A | 108.6 | C19—C18—C17 | 120.0 |
C3—C4—H4A | 108.6 | C19—C18—O4 | 116.4 (3) |
C5—C4—H4B | 108.6 | C17—C18—O4 | 123.6 (3) |
C3—C4—H4B | 108.6 | C18—C19—C20 | 120.0 |
H4A—C4—H4B | 107.6 | C18—C19—H19A | 120.0 |
O1—C5—C6 | 120.8 (2) | C20—C19—H19A | 120.0 |
O1—C5—C4 | 119.8 (2) | C19—C20—C15 | 120.0 |
C6—C5—C4 | 119.5 (2) | C19—C20—H20A | 120.0 |
C1—C6—C5 | 119.9 (2) | C15—C20—H20A | 120.0 |
C1—C6—C7 | 121.2 (2) | C21—O4—C18 | 120.7 (3) |
C5—C6—C7 | 118.9 (2) | O4—C21—F2 | 107.8 (6) |
C6—C7—C15 | 113.7 (3) | O4—C21—F1 | 107.6 (5) |
C6—C7—C8 | 110.86 (19) | F2—C21—F1 | 118.1 (5) |
C15—C7—C8 | 112.6 (3) | O4—C21—H21A | 107.6 |
C6—C7—C15A | 105.9 (4) | F2—C21—H21A | 107.6 |
C8—C7—C15A | 108.7 (4) | F1—C21—H21A | 107.6 |
C6—C7—H7 | 107.8 (15) | C16A—C15A—C20A | 120.0 |
C15—C7—H7 | 102.1 (15) | C16A—C15A—C7 | 121.6 (4) |
C8—C7—H7 | 109.2 (15) | C20A—C15A—C7 | 118.3 (4) |
C15A—C7—H7 | 114.3 (16) | C17A—C16A—C15A | 120.0 |
C9—C8—C13 | 120.4 (2) | C17A—C16A—H16B | 120.0 |
C9—C8—C7 | 121.2 (2) | C15A—C16A—H16B | 120.0 |
C13—C8—C7 | 118.4 (2) | C16A—C17A—C18A | 120.0 |
C8—C9—N1 | 119.6 (2) | C16A—C17A—H17B | 120.0 |
C8—C9—C12 | 127.0 (3) | C18A—C17A—H17B | 120.0 |
N1—C9—C12 | 113.4 (2) | C19A—C18A—C17A | 120.0 |
C3—C10—H10A | 109.5 | C19A—C18A—O4A | 120.3 (4) |
C3—C10—H10B | 109.5 | C17A—C18A—O4A | 119.5 (4) |
H10A—C10—H10B | 109.5 | C18A—C19A—C20A | 120.0 |
C3—C10—H10C | 109.5 | C18A—C19A—H19B | 120.0 |
H10A—C10—H10C | 109.5 | C20A—C19A—H19B | 120.0 |
H10B—C10—H10C | 109.5 | C19A—C20A—C15A | 120.0 |
C3—C11—H11A | 109.5 | C19A—C20A—H20B | 120.0 |
C3—C11—H11B | 109.5 | C15A—C20A—H20B | 120.0 |
H11A—C11—H11B | 109.5 | C21A—O4A—C18A | 119.8 (5) |
C3—C11—H11C | 109.5 | O4A—C21A—F2A | 110.1 (7) |
H11A—C11—H11C | 109.5 | O4A—C21A—F1A | 101.2 (6) |
H11B—C11—H11C | 109.5 | F2A—C21A—F1A | 121.3 (7) |
C9—C12—H12A | 109.5 | O4A—C21A—H21B | 107.8 |
C9—C12—H12B | 109.5 | F2A—C21A—H21B | 107.8 |
H12A—C12—H12B | 109.5 | F1A—C21A—H21B | 107.8 |
C9—C12—H12C | 109.5 | ||
C9—N1—C1—C6 | 10.0 (4) | C9—C8—C13—O2 | 1.7 (4) |
C9—N1—C1—C2 | −167.7 (2) | C7—C8—C13—O2 | −175.6 (3) |
C6—C1—C2—C3 | 28.0 (4) | C9—C8—C13—O3 | −177.0 (2) |
N1—C1—C2—C3 | −154.2 (2) | C7—C8—C13—O3 | 5.7 (3) |
C1—C2—C3—C4 | −51.7 (3) | C6—C7—C15—C16 | −74.8 (3) |
C1—C2—C3—C10 | −171.3 (3) | C8—C7—C15—C16 | 52.4 (4) |
C1—C2—C3—C11 | 69.1 (3) | C6—C7—C15—C20 | 108.0 (3) |
C10—C3—C4—C5 | 169.0 (2) | C8—C7—C15—C20 | −124.8 (3) |
C2—C3—C4—C5 | 49.9 (3) | C20—C15—C16—C17 | 0.0 |
C11—C3—C4—C5 | −71.1 (3) | C7—C15—C16—C17 | −177.2 (4) |
C3—C4—C5—O1 | 158.9 (2) | C15—C16—C17—C18 | 0.0 |
C3—C4—C5—C6 | −23.1 (3) | C16—C17—C18—C19 | 0.0 |
N1—C1—C6—C5 | −176.0 (2) | C16—C17—C18—O4 | 179.9 (4) |
C2—C1—C6—C5 | 1.6 (4) | C17—C18—C19—C20 | 0.0 |
N1—C1—C6—C7 | 4.5 (4) | O4—C18—C19—C20 | −179.9 (3) |
C2—C1—C6—C7 | −177.9 (2) | C18—C19—C20—C15 | 0.0 |
O1—C5—C6—C1 | 173.5 (2) | C16—C15—C20—C19 | 0.0 |
C4—C5—C6—C1 | −4.5 (3) | C7—C15—C20—C19 | 177.1 (4) |
O1—C5—C6—C7 | −7.0 (4) | C19—C18—O4—C21 | 155.4 (5) |
C4—C5—C6—C7 | 175.0 (2) | C17—C18—O4—C21 | −24.5 (6) |
C1—C6—C7—C15 | 110.1 (3) | C18—O4—C21—F2 | −51.8 (7) |
C5—C6—C7—C15 | −69.4 (3) | C18—O4—C21—F1 | 76.6 (6) |
C1—C6—C7—C8 | −18.1 (3) | C6—C7—C15A—C16A | −64.9 (6) |
C5—C6—C7—C8 | 162.4 (2) | C8—C7—C15A—C16A | 54.3 (6) |
C1—C6—C7—C15A | 99.6 (4) | C6—C7—C15A—C20A | 118.7 (4) |
C5—C6—C7—C15A | −79.9 (4) | C8—C7—C15A—C20A | −122.1 (4) |
C6—C7—C8—C9 | 20.0 (3) | C20A—C15A—C16A—C17A | 0.0 |
C15—C7—C8—C9 | −108.7 (3) | C7—C15A—C16A—C17A | −176.4 (8) |
C15A—C7—C8—C9 | −96.0 (4) | C15A—C16A—C17A—C18A | 0.0 |
C6—C7—C8—C13 | −162.7 (2) | C16A—C17A—C18A—C19A | 0.0 |
C15—C7—C8—C13 | 68.6 (3) | C16A—C17A—C18A—O4A | −175.9 (6) |
C15A—C7—C8—C13 | 81.3 (4) | C17A—C18A—C19A—C20A | 0.0 |
C13—C8—C9—N1 | 174.5 (2) | O4A—C18A—C19A—C20A | 175.9 (6) |
C7—C8—C9—N1 | −8.2 (4) | C18A—C19A—C20A—C15A | 0.0 |
C13—C8—C9—C12 | −5.2 (4) | C16A—C15A—C20A—C19A | 0.0 |
C7—C8—C9—C12 | 172.0 (2) | C7—C15A—C20A—C19A | 176.5 (8) |
C1—N1—C9—C8 | −8.1 (4) | C19A—C18A—O4A—C21A | 75.5 (8) |
C1—N1—C9—C12 | 171.7 (2) | C17A—C18A—O4A—C21A | −108.6 (7) |
C14—O3—C13—O2 | −2.9 (4) | C18A—O4A—C21A—F2A | −66.7 (9) |
C14—O3—C13—C8 | 175.9 (2) | C18A—O4A—C21A—F1A | 62.8 (8) |