F1—C24 | 1.3658 (18) | C7A—C8A | 1.525 (16) |
F2—C24 | 1.3510 (19) | C7A—H7AA | 0.9900 |
O1—C5 | 1.2374 (18) | C7A—H7AB | 0.9900 |
O2—C24 | 1.3449 (19) | C8A—C9 | 1.553 (18) |
O2—C21 | 1.4107 (17) | C8A—H8AA | 0.9900 |
O3—C13 | 1.2127 (19) | C8A—H8AB | 0.9900 |
O4—C13 | 1.3490 (18) | C11A—H11D | 0.9800 |
O4—C14 | 1.4757 (17) | C11A—H11E | 0.9800 |
N1—C9 | 1.3692 (18) | C11A—H11F | 0.9800 |
N1—C1 | 1.3902 (18) | C12A—H12D | 0.9800 |
N1—H1N | 0.88 (2) | C12A—H12E | 0.9800 |
C1—C2 | 1.3578 (19) | C12A—H12F | 0.9800 |
C1—C10 | 1.501 (2) | C10—H10A | 0.9800 |
C2—C13 | 1.470 (2) | C10—H10B | 0.9800 |
C2—C3 | 1.5273 (19) | C10—H10C | 0.9800 |
C3—C4 | 1.5132 (18) | C14—C16 | 1.511 (3) |
C3—C18 | 1.531 (2) | C14—C17 | 1.512 (2) |
C3—H3A | 1.0000 | C14—C15 | 1.512 (2) |
C4—C9 | 1.364 (2) | C15—H15A | 0.9800 |
C4—C5 | 1.449 (2) | C15—H15B | 0.9800 |
C5—C6 | 1.5295 (19) | C15—H15C | 0.9800 |
C6—C7A | 1.447 (4) | C16—H16A | 0.9800 |
C6—C12 | 1.510 (3) | C16—H16B | 0.9800 |
C6—C11A | 1.546 (5) | C16—H16C | 0.9800 |
C6—C7 | 1.559 (3) | C17—H17A | 0.9800 |
C6—C11 | 1.560 (3) | C17—H17B | 0.9800 |
C6—C12A | 1.570 (4) | C17—H17C | 0.9800 |
C7—C8 | 1.547 (10) | C18—C19 | 1.3918 (19) |
C7—H7A | 0.9900 | C18—C23 | 1.396 (2) |
C7—H7B | 0.9900 | C19—C20 | 1.398 (2) |
C8—C9 | 1.468 (11) | C19—H19A | 0.9500 |
C8—H8A | 0.9900 | C20—C21 | 1.380 (2) |
C8—H8B | 0.9900 | C20—H20A | 0.9500 |
C11—H11A | 0.9800 | C21—C22 | 1.386 (2) |
C11—H11B | 0.9800 | C22—C23 | 1.394 (2) |
C11—H11C | 0.9800 | C22—H22A | 0.9500 |
C12—H12A | 0.9800 | C23—H23A | 0.9500 |
C12—H12B | 0.9800 | C24—H24A | 1.0000 |
C12—H12C | 0.9800 | ||
C24—O2—C21 | 121.96 (12) | H11D—C11A—H11E | 109.5 |
C13—O4—C14 | 122.42 (12) | C6—C11A—H11F | 109.5 |
C9—N1—C1 | 122.21 (12) | H11D—C11A—H11F | 109.5 |
C9—N1—H1N | 117.9 (13) | H11E—C11A—H11F | 109.5 |
C1—N1—H1N | 116.2 (13) | C6—C12A—H12D | 109.5 |
C2—C1—N1 | 119.02 (13) | C6—C12A—H12E | 109.5 |
C2—C1—C10 | 129.03 (13) | H12D—C12A—H12E | 109.5 |
N1—C1—C10 | 111.95 (12) | C6—C12A—H12F | 109.5 |
C1—C2—C13 | 125.87 (13) | H12D—C12A—H12F | 109.5 |
C1—C2—C3 | 119.37 (12) | H12E—C12A—H12F | 109.5 |
C13—C2—C3 | 114.74 (12) | C4—C9—N1 | 119.68 (13) |
C4—C3—C2 | 109.63 (11) | C4—C9—C8 | 125.1 (4) |
C4—C3—C18 | 110.75 (11) | N1—C9—C8 | 115.2 (4) |
C2—C3—C18 | 111.59 (11) | C4—C9—C8A | 120.9 (7) |
C4—C3—H3A | 108.3 | N1—C9—C8A | 119.4 (7) |
C2—C3—H3A | 108.3 | C1—C10—H10A | 109.5 |
C18—C3—H3A | 108.3 | C1—C10—H10B | 109.5 |
C9—C4—C5 | 120.75 (13) | H10A—C10—H10B | 109.5 |
C9—C4—C3 | 119.19 (12) | C1—C10—H10C | 109.5 |
C5—C4—C3 | 119.94 (12) | H10A—C10—H10C | 109.5 |
O1—C5—C4 | 121.30 (13) | H10B—C10—H10C | 109.5 |
O1—C5—C6 | 119.73 (13) | O3—C13—O4 | 123.28 (14) |
C4—C5—C6 | 118.97 (12) | O3—C13—C2 | 122.98 (14) |
C7A—C6—C5 | 111.51 (19) | O4—C13—C2 | 113.70 (12) |
C12—C6—C5 | 113.18 (14) | O4—C14—C16 | 102.37 (13) |
C7A—C6—C11A | 114.0 (3) | O4—C14—C17 | 111.14 (12) |
C5—C6—C11A | 107.99 (19) | C16—C14—C17 | 109.82 (14) |
C12—C6—C7 | 109.13 (15) | O4—C14—C15 | 109.50 (13) |
C5—C6—C7 | 111.51 (13) | C16—C14—C15 | 111.71 (19) |
C12—C6—C11 | 109.71 (17) | C17—C14—C15 | 111.91 (17) |
C5—C6—C11 | 104.16 (13) | C14—C15—H15A | 109.5 |
C7—C6—C11 | 108.97 (16) | C14—C15—H15B | 109.5 |
C7A—C6—C12A | 114.1 (3) | H15A—C15—H15B | 109.5 |
C5—C6—C12A | 101.5 (2) | C14—C15—H15C | 109.5 |
C11A—C6—C12A | 106.9 (3) | H15A—C15—H15C | 109.5 |
C8—C7—C6 | 112.2 (4) | H15B—C15—H15C | 109.5 |
C8—C7—H7A | 109.2 | C14—C16—H16A | 109.5 |
C6—C7—H7A | 109.2 | C14—C16—H16B | 109.5 |
C8—C7—H7B | 109.2 | H16A—C16—H16B | 109.5 |
C6—C7—H7B | 109.2 | C14—C16—H16C | 109.5 |
H7A—C7—H7B | 107.9 | H16A—C16—H16C | 109.5 |
C9—C8—C7 | 111.1 (7) | H16B—C16—H16C | 109.5 |
C9—C8—H8A | 109.4 | C14—C17—H17A | 109.5 |
C7—C8—H8A | 109.4 | C14—C17—H17B | 109.5 |
C9—C8—H8B | 109.4 | H17A—C17—H17B | 109.5 |
C7—C8—H8B | 109.4 | C14—C17—H17C | 109.5 |
H8A—C8—H8B | 108.0 | H17A—C17—H17C | 109.5 |
C6—C11—H11A | 109.5 | H17B—C17—H17C | 109.5 |
C6—C11—H11B | 109.5 | C19—C18—C23 | 117.70 (13) |
H11A—C11—H11B | 109.5 | C19—C18—C3 | 121.64 (13) |
C6—C11—H11C | 109.5 | C23—C18—C3 | 120.65 (12) |
H11A—C11—H11C | 109.5 | C18—C19—C20 | 121.21 (14) |
H11B—C11—H11C | 109.5 | C18—C19—H19A | 119.4 |
C6—C12—H12A | 109.5 | C20—C19—H19A | 119.4 |
C6—C12—H12B | 109.5 | C21—C20—C19 | 119.40 (13) |
H12A—C12—H12B | 109.5 | C21—C20—H20A | 120.3 |
C6—C12—H12C | 109.5 | C19—C20—H20A | 120.3 |
H12A—C12—H12C | 109.5 | C20—C21—C22 | 121.11 (14) |
H12B—C12—H12C | 109.5 | C20—C21—O2 | 114.03 (13) |
C6—C7A—C8A | 112.7 (8) | C22—C21—O2 | 124.86 (14) |
C6—C7A—H7AA | 109.0 | C21—C22—C23 | 118.53 (14) |
C8A—C7A—H7AA | 109.0 | C21—C22—H22A | 120.7 |
C6—C7A—H7AB | 109.0 | C23—C22—H22A | 120.7 |
C8A—C7A—H7AB | 109.0 | C22—C23—C18 | 122.05 (14) |
H7AA—C7A—H7AB | 107.8 | C22—C23—H23A | 119.0 |
C7A—C8A—C9 | 110.2 (11) | C18—C23—H23A | 119.0 |
C7A—C8A—H8AA | 109.6 | O2—C24—F2 | 112.74 (14) |
C9—C8A—H8AA | 109.6 | O2—C24—F1 | 111.38 (12) |
C7A—C8A—H8AB | 109.6 | F2—C24—F1 | 105.20 (13) |
C9—C8A—H8AB | 109.6 | O2—C24—H24A | 109.1 |
H8AA—C8A—H8AB | 108.1 | F2—C24—H24A | 109.1 |
C6—C11A—H11D | 109.5 | F1—C24—H24A | 109.1 |
C6—C11A—H11E | 109.5 | ||
C9—N1—C1—C2 | 16.6 (2) | C3—C4—C9—N1 | −10.2 (2) |
C9—N1—C1—C10 | −162.96 (12) | C5—C4—C9—C8 | −5.5 (5) |
N1—C1—C2—C13 | −168.52 (13) | C3—C4—C9—C8 | 170.5 (5) |
C10—C1—C2—C13 | 10.9 (2) | C5—C4—C9—C8A | −9.4 (8) |
N1—C1—C2—C3 | 9.82 (19) | C3—C4—C9—C8A | 166.6 (8) |
C10—C1—C2—C3 | −170.73 (13) | C1—N1—C9—C4 | −16.5 (2) |
C1—C2—C3—C4 | −32.19 (17) | C1—N1—C9—C8 | 162.9 (4) |
C13—C2—C3—C4 | 146.33 (12) | C1—N1—C9—C8A | 166.7 (8) |
C1—C2—C3—C18 | 90.88 (15) | C7—C8—C9—C4 | 26.3 (8) |
C13—C2—C3—C18 | −90.60 (14) | C7—C8—C9—N1 | −153.0 (4) |
C2—C3—C4—C9 | 32.34 (18) | C7A—C8A—C9—C4 | −19.0 (15) |
C18—C3—C4—C9 | −91.22 (16) | C7A—C8A—C9—N1 | 157.8 (7) |
C2—C3—C4—C5 | −151.65 (13) | C14—O4—C13—O3 | −1.5 (2) |
C18—C3—C4—C5 | 84.79 (16) | C14—O4—C13—C2 | 176.23 (12) |
C9—C4—C5—O1 | −174.39 (14) | C1—C2—C13—O3 | −176.94 (15) |
C3—C4—C5—O1 | 9.7 (2) | C3—C2—C13—O3 | 4.6 (2) |
C9—C4—C5—C6 | 6.6 (2) | C1—C2—C13—O4 | 5.3 (2) |
C3—C4—C5—C6 | −169.33 (12) | C3—C2—C13—O4 | −173.09 (12) |
O1—C5—C6—C7A | −152.9 (2) | C13—O4—C14—C16 | 176.95 (15) |
C4—C5—C6—C7A | 26.1 (2) | C13—O4—C14—C17 | 59.76 (18) |
O1—C5—C6—C12 | 28.8 (2) | C13—O4—C14—C15 | −64.4 (2) |
C4—C5—C6—C12 | −152.19 (17) | C4—C3—C18—C19 | −134.72 (14) |
O1—C5—C6—C11A | −26.9 (3) | C2—C3—C18—C19 | 102.85 (15) |
C4—C5—C6—C11A | 152.1 (2) | C4—C3—C18—C23 | 46.27 (18) |
O1—C5—C6—C7 | 152.31 (15) | C2—C3—C18—C23 | −76.16 (16) |
C4—C5—C6—C7 | −28.68 (19) | C23—C18—C19—C20 | −0.2 (2) |
O1—C5—C6—C11 | −90.31 (18) | C3—C18—C19—C20 | −179.23 (13) |
C4—C5—C6—C11 | 88.70 (17) | C18—C19—C20—C21 | 0.9 (2) |
O1—C5—C6—C12A | 85.2 (2) | C19—C20—C21—C22 | −0.8 (2) |
C4—C5—C6—C12A | −95.7 (2) | C19—C20—C21—O2 | 178.96 (13) |
C12—C6—C7—C8 | 174.7 (4) | C24—O2—C21—C20 | 168.08 (14) |
C5—C6—C7—C8 | 48.9 (4) | C24—O2—C21—C22 | −12.1 (2) |
C11—C6—C7—C8 | −65.5 (4) | C20—C21—C22—C23 | 0.1 (2) |
C6—C7—C8—C9 | −47.3 (6) | O2—C21—C22—C23 | −179.67 (14) |
C5—C6—C7A—C8A | −55.3 (8) | C21—C22—C23—C18 | 0.6 (2) |
C11A—C6—C7A—C8A | −177.9 (8) | C19—C18—C23—C22 | −0.6 (2) |
C12A—C6—C7A—C8A | 58.9 (9) | C3—C18—C23—C22 | 178.48 (14) |
C6—C7A—C8A—C9 | 52.0 (13) | C21—O2—C24—F2 | 60.27 (18) |
C5—C4—C9—N1 | 173.81 (13) | C21—O2—C24—F1 | −57.73 (18) |