| Crystal data |
| Chemical formula |
C31H24N4O2
|
|
M
r
|
484.54 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c (Å) |
8.8038 (6), 10.2277 (7), 14.0937 (10) |
| α, β, γ (°) |
90.262 (1), 96.630 (1), 108.395 (1) |
|
V (Å3) |
1195.00 (14) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.09 |
| Crystal size (mm) |
0.41 × 0.34 × 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEX CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.84, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
22697, 6292, 4672 |
|
R
int
|
0.029 |
| (sin θ/λ)max (Å−1) |
0.685 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.129, 1.02 |
| No. of reflections |
6292 |
| No. of parameters |
430 |
| H-atom treatment |
All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) |
0.40, −0.22 |
