| Crystal data |
| Chemical formula |
[SmNa(C8H7O3)4][+solvent] |
|
M
r
|
777.88 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
11.5512 (7), 24.4768 (14), 12.8355 (6) |
| β (°) |
115.742 (2) |
|
V (Å3) |
3268.9 (3) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.87 |
| Crystal size (mm) |
0.05 × 0.01 × 0.002 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture with photon detector |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
41476, 6204, 4562 |
|
R
int
|
0.147 |
| (sin θ/λ)max (Å−1) |
0.610 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.050, 0.108, 1.02 |
| No. of reflections |
6204 |
| No. of parameters |
419 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.76, −1.13 |
