|
2
|
C13—H13⋯O2i
|
0.93 |
2.50 |
3.097 (4) |
122.5 |
(i) −x, −y + 1, −z + 1 |
| C14—H14⋯O)i
|
0.93 |
2.55 |
3.118 (4) |
120.2 |
| C15—H15⋯O4ii
|
0.93 |
2.36 |
3.232 (4) |
156.0 |
(ii) −x + 1, −y + 1, −z + 1 |
| N2—H2B⋯O3iii
|
0.86 |
2.24 |
2.910 (3) |
135.2 |
(iii) −x, −y + 2, −z + 1 |
| N2—H2A⋯O3iv
|
0.86 |
2.04 |
2.895 (4) |
173.8 |
(iv) x + 2, y, z + 1 |
| O4—H4⋯N1v
|
0.82 |
1.78 |
2.577 (4) |
164.8 |
(v) x − 2, y, z − 1 |
|
3
|
N2—H2B⋯O2i
|
0.86 |
2.16 |
2.9669 (16) |
155.6 |
(i) x + 1/2, y − 1/2, z
|
| N2—H2B⋯O3i
|
0.86 |
2.28 |
2.8755 (14) |
126.6 |
| C12—H12⋯O2i
|
0.93 |
2.46 |
3.2087(16) |
138.1 |
| C8—H8⋯O1ii
|
0.93 |
2.60 |
3.5228 (16) |
170.4 |
(ii) −x + 1/2, y + 1/2, −z + 3/2 |
| N2—H2A⋯O3iii
|
0.86 |
2.08 |
2.9292 (15) |
168.4 |
(iii) −x + 1, −y, −z + 1 |
|
4
|
C16—H16B⋯O4i
|
0.96 |
2.62 |
3.533 (3) |
158.8 |
(i) −x + 1, y + 1/2, −z + 1/2 |
| O3—H3A⋯N1ii
|
0.82 |
1.86 |
2.658 (2) |
165.1 |
(ii) −x + 1, y − 1/2, −z + 3/2 |
| C12—H12⋯O2iii
|
0.93 |
2.62 |
3.425 (3) |
144.8 |
(iii) x + 1, −y + 1/2, z + 1/2 |
| C16—H16A⋯O3iv
|
0.96 |
2.60 |
3.410 (3) |
141.8 |
(iv) −x + 1, y + 1/2, −z + 3/2 |
| N2—H2A⋯O4iii
|
0.89 (3) |
2.01 (3) |
2.817 (3) |
150 (2) |
(iii) x + 1, −y + 1/2, z + 1/2 |
|
5
|
O4—H4A⋯O6i
|
0.82 |
1.85 |
2.6581 (14) |
167.5 |
(i) −x, −y, −z + 2 |
| O5—H5A⋯O3ii
|
0.82 |
1.84 |
2.6417 (14) |
166.9 |
| N1—H1B⋯O6ii
|
0.86 |
2.58 |
3.4143 (17) |
163.4 |
(ii) −x + 1/2, y + 1/2, −z + 5/2 |
| C16—H16⋯O1iii
|
0.93 |
2.55 |
3.4789 (16) |
174.5 |
(iii) −x + 1, −y + 1, −z + 2 |
| N1—H1A⋯O2iii
|
0.86 |
2.32 |
3.1762 (16) |
176.0 |
|
6
|
O4—H4⋯N2i
|
0.82 |
1.90 |
2.675 (9) |
157.0 |
(i) −x + 1/2, y − 1/2, z − 1/2 |
| C8—H8⋯O3ii
|
0.93 |
2.59 |
3.334 (12) |
137.7 |
(ii) −x + 1, −y, z + 1/2 |
| N4—H4A⋯O3iii
|
1.04 (11) |
1.80 (11) |
2.799 (11) |
160 (8) |
(iii) x + 1/2, y + 1/2, z + 1/2 |
| N4—H4B⋯N1iv
|
0.87 (11) |
2.23 (11) |
3.067 (9) |
163 (9) |
(iv) −x + 1/2, y + 1/2, z − 1/2 |
| N3—H3A⋯O2 |
0.72 (11) |
2.51 (11) |
2.957 (11) |
121 (10) |
|
| N3—H3A⋯O4 |
0.72 (11) |
2.00 (12) |
2.686 (11) |
158 (11) |
|