Table 3.
Methylation analysis data of SUSP-4.
| Retention time (min) | Methylated sugar | Mass fragments (m/z) | Area (%) | Type of linkage |
|---|---|---|---|---|
| 9.623 | 2,3,5-Me3-Araf | 43, 71, 87, 101, 117, 129, 145, and 161 | 1.80 | Araf-1 |
| 10.915 | 2,3,4-Me3-Rhap | 43, 72, 89, 101, 115, 117, 131, 161, and 175 | 0.48 | Rhap-1 |
| 11.081 | 2,3,4-Me3-Xylp | 43, 87, 101, 117, 131, 161, 173, 205 | 1.04 | Xylp-1 |
| 12.196 | 2,3,4-Me3-Fucp | 43, 72, 89, 101, 115, 117, 131, 161, and 175 | 0.21 | Fucp-1 |
| 14.784 | 2,3-Me2-Araf | 43, 87, 99, 101, 117, 129, and 189 | 8.39 | Araf-1-5 |
| 15.076 | 2,3-Me2-Xylp | 43, 87, 101, 117, 129, 161, and 189 | 4.71 | Xylp-1-4 |
| 15.390 | 2,4-Me2-Fucp | 43, 89, 101, 117, 131, 159, 173, and 233 | 1.23 | Fucp-1-3 |
| 16.621 | 2,3,4,6-Me4-Glcp | 43, 71, 87, 101, 117, 129, 145, 161, and 205 | 2.83 | Glcp-1 |
| 17.871 | 2,3,4,6-Me4-Galp | 43, 71, 87, 101, 117, 129, 145, 161, 205 | 5.41 | Galp-1 |
| 19.233 | 3-Me1-Rhap | 43, 87, 101, 117, 129, 143, 159, 189, and 203 | 3.41 | Rhap-1-2-4 |
| 19.441 | 3-Me1-Araf | 43, 85, 99, 117, 127, 131, 159, 201, and 261 | 2.35 | Araf-1-2-5 |
| 20.964 | 3,4,6-Me3-Manp | 43, 71, 87, 99, 101, 129, 145, 161, and 189 | 3.05 | Manp-1-2 |
| 21.329 | 2,3,4-Me3-Galp | 43, 71, 87, 99, 101, 117, 129, 161, 173, 189, and 233 | 5.25 | Galp-1-6 |
| 21.666 | 2,3,6-Me3-Galp | 43, 71, 87, 99, 101, 113, 117, 129, 131, 161, 173, and 233 | 35.62 | Galp-1-4 |
| 21.923 | 2,3,6-Me3-Glcp | 43, 71, 87, 99, 101, 113, 117, 129, 131, 161, 173, and 233 | 6.72 | Glcp-1-4 |
| 22.710 | 2,4,6-Me3-Galp | 43, 71, 87, 101, 117, 129, 161, 173, and 233 | 1.54 | Galp-1-3 |
| 25.445 | 2,6-Me2-Galp | 43, 87, 97, 117, 129, 143, 159, and 185 | 11.84 | Galp-1-3-4 |
| 26.572 | 3,4–Me2-Manp | 43, 87, 99, 113, 129, 173, 189, and 233 | 2.83 | Manp-1-2-6 |
| 28.432 | 2,3-Me2-Glcp | 43, 85, 99, 101, 117, 127, 142, 159, 201, and 261 | 1.29 | Glcp-1-4-6 |