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. 2023 Aug 10;14(2):177–195. doi: 10.1016/j.jpha.2023.08.003

Table 4.

Chemical shifts of resonances in 1H nuclear magnetic resonance (NMR) and13C NMR of SUSP-4.

Signals Glycosyl residues H1/C1 H2/C2 H3/C3 H4/C4 H5/C5 C6/H6a,b
A α-l-Araf-(1→ 5.01 4.01 3.84 3.92 3.70 3.37
108.80 82.70 77.80 85.10 62.30
B →5)-α-l-Araf-(1→ 5.05 4.07 3.94 4.15 3.81 3.71
108.90 82.20 78.10 83.70 68.30
C →2,5)-α-l-Araf-(1→ 5.11 4.09 4.19 3.94 3.81
107.80 88.50 78.30 83.80 68.30
D →6)-β-d-Galp-(1→ 4.38 3.45 3.59 3.87 3.89 3.96 3.83
104.90 72.20 73.90 75.00 69.90 70.50
E β-d-Galp-(1→ 4.51 3.29 3.47 3.22 3.61 3.55 3.45
104.50 74.70 76.60 83.40 77.40 64.00
F →4)-α-d-GalAp-(1→ 4.98 3.68 3.94 3.68 3.73
100.40 69.40 70.10 78.10 72.70 176.70 54.10
G →3,4)-α-d-GalAp-(1→ 4.84 4.18 4.10 3.67
101.40 72.70 82.60 78.10 71.80 176.70
H →4)-β-d-Xylp-(1→ 4.35 3.23 3.50 3.71 4.04 3.32
103.00 74.00 75.00 77.70 64.30
I →2,4)-α-l-Rha-(1→ 5.16 4.06 3.84 3.61 3.76 1.23
99.80 77.70 70.30 76.80 69.70 18.20