Table 1.
Analytical performance data of the calibration graphs for the determination of FVM, and IVM by the proposed methods
| Analyte | FVM | IVM | ||||
|---|---|---|---|---|---|---|
| Method | FFZD | FFR | DWZ | FFZD | FFR | DWZ |
| Wavelength (nm) | 270 | 272–258 | ∆A 270–290 | 240 | 254–291 | ∆A 245–260 |
| Linearity range (µg/mL) | 5–40 | 2.5–25 | ||||
| LOD (µg/mL)a | 0.7352 | 1.5306 | 0.4202 | 0.3995 | 0.0980 | 0.1213 |
| LOQ (µg/mL)b | 2.2279 | 4.6381 | 1.2732 | 1.2106 | 0.2971 | 0.3677 |
| Regression coefficient | 0.99929 | 0.99966 | 0.99963 | 0.99947 | 0.99997 | 0.99995 |
| Slope | 0.0025 | 0.2521 | 0.0145 | 0.0008 | 0.0483 | 0.0350 |
| SE of slope | 0.0001 | 0.0114 | 0.0002 | 0.00001 | 0.0002 | 0.0002 |
| Intercept | − 0.0011 | 0.2284 | 0.0130 | 0.0001 | -0.0249 | 0.0005 |
| SE of intercept | 0.0006 | 0.1169 | 0.0019 | 0.0001 | 0.0014 | 0.0013 |
aLimit of detection
bLimit of quantitation