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. 2024 Feb 27;26(9):1975–1979. doi: 10.1021/acs.orglett.4c00513

Table 3. Photodetosylation of N-Ts Aniline.

graphic file with name ol4c00513_0008.jpg

entry DHP equiv of Cs2CO3 ΔGBET (eV) yield of 21a (%)
1 I 5.0 –2.02 22
2 IV 5.0 –2.34 33
3 IV 2.0 –2.34 53b
a

Yields calculated by 1H NMR using 1,3,5-trimethoxybenzene as an external standard.

b

Isolated yield.