| Thermogravimetric analysis |
The thermal stability of yolk–shell microgels was explored |
P(MAA-co-EGDMA)@void@P(NIPAM-co-MAA) |
48
|
| Fe3O4@void@PMAA |
30
|
| Fe3O4@void@PMAA@void@PNIPAM |
54
|
| Energy dispersive X-ray (EDX) analysis |
Mass content of metal in hybrid yolk–shell microgels was discovered |
Ag@air@PMAA |
75
|
| X-ray photoelectron spectroscopy (XPS) |
Concentration of metal in hybrid yolk–shell microgels was predicted |
PS@void@PS-co-PMAA |
77
|
| Fe3O4@void@PMAA@void@PNIPAM |
54
|
| Vibrating-sample magnetometry (VSM) |
To determine the saturation magnetization of magnetic particles, present in yolk–shell microgels |
Fe3O4@void@PMAA |
78
|
| SiO2–Fe3O4@void@P(BIS-co-MAA) |
71
|
| X-ray diffraction (XRD) spectroscopy |
To determine the size of the nanostructure |
Fe3O4@void@PMAA@void@PNIPAM |
54
|
| To determine the crystal structure of nanoparticles of the yolk–shell hybrid. Microgels |
| Dynamic light scattering (DLS) |
To determine the Dh of yolk–shell microgels in swollen and de-swollen state |
Au@void@PNIPAM |
46
|
| PMAA@void@PNIPAM |
50
|
| P(MAA-co-EDGMA)@void@PNIPAM |
49
|
| To determine the size distribution of microgels |
SiO2–Fe3O4@void@P(BIS-co-MAA) |
71
|
| Fe3O4@void@PMAA |
79
|
| Fourier transform infrared (FT-IR) spectroscopy |
To determine the bonds present in the network of hybrid yolk–shell microgels |
Ag@void@PMAA |
75
|
| CPMAA@void@CPNIPAM |
72
|
| Fe3O4@void@PMAA |
78
|
| Fe3O4@void@PMAA@void@PNIPAM |
54
|
| Au–Fe3O4@void@PNIPAM |
80
|
| Fe3O4@void@PMAA |
30
|
| Scanning electron microscopy (SEM) |
To determine the morphology of hybrid yolk–shell microgels |
Fe3O4@void@PMAA |
78
|
| UV-visible spectroscopy |
To determine the optical properties of hybrid yolk–shell microgels |
CPMAA@void@CPNIPAM |
72
|
| The dimensions of nanostructures were predicted |
| Transmission electron microscopy (TEM) |
The shape and size distribution of hybrid yolk–shell microgels was investigated |
P(MAA-co-EGDMA)@void@P(NIPAM-co-MAA) |
48
|
| PMAA@void@PNIPAM |
50
|
| Au–Fe3O4@void@PNIPAM |
80
|
| SiO2–Fe3O4@void@P(BIS-co-MAA) |
71
|