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Standard conditions follow Table 1, entry 1. Yields of isolated products. See ESI for experimental procedures.
NMR yield.
Olefin (1 equiv.) and green light (510–575 nm).
Using trans-3-hexene. With cis-3-hexene, 39 was obtained in 88% yield and 15 : 1 syn/anti.
Catalyst PC2 (1 mol%).
Catalyst PC3 (1 mol%).
DMSO as solvent or cosolvent.
Mixture of regioisomers, see ESI.
