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| Std order | Run order | Catalyst | FeCl2 (mL) | H2O2 (mL) | Yield of methanol (μmol h−1 gcat−1) |
|---|---|---|---|---|---|
| 5 | R1 | Ti-A | 0.0 | 1.0 | 0.6440 |
| 1 | R2 | Ti-A | 0.0 | 0.0 | 0.5224 |
| 6 | R3 | Ti-B | 0.0 | 1.0 | 0.2242 |
| 10 | R4 | Ti-B | 7.5 | 0.5 | 0.4251 |
| 7 | R5 | Ti-A | 15.0 | 1.0 | 0.7257 |
| 4 | R6 | Ti-B | 15.0 | 0.0 | 0.3901 |
| 3 | R7 | Ti-A | 15.0 | 0.0 | 0.4935 |
| 2 | R8 | Ti-B | 0.0 | 0.0 | 0.3501 |
| 8 | R9 | Ti-B | 15.0 | 1.0 | 0.3705 |
| 9 | R10 | Ti-A | 7.5 | 0.5 | 0.6679 |
