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. 2024 Mar 8;5(1):102933. doi: 10.1016/j.xpro.2024.102933

Synthesis of the heterogeneous catalyst 18

Reagent Concentration Amount
Merrifield resin 0.204 mmol 200 mg
tert-butyl (S)-(1-(butylamino)-3-(4-hydroxyphenyl)-1-oxopropan-2-yl)carbamate 16 0.24 mmol 100 mg
Potassium iodide 0.02 mmol 3.4 mg
Sodium hydride (60% in mineral oil) 0.31 mmol 12 mg
N,N-dimethylformamide 0.051 M 4 mL