Synthesis of the heterogeneous catalyst 18
| Reagent | Concentration | Amount |
|---|---|---|
| Merrifield resin | 0.204 mmol | 200 mg |
| tert-butyl (S)-(1-(butylamino)-3-(4-hydroxyphenyl)-1-oxopropan-2-yl)carbamate 16 | 0.24 mmol | 100 mg |
| Potassium iodide | 0.02 mmol | 3.4 mg |
| Sodium hydride (60% in mineral oil) | 0.31 mmol | 12 mg |
| N,N-dimethylformamide | 0.051 M | 4 mL |