Figure 3.

a) Schematic model of M₆L₆ circular helicate indicating the three distinct Gd⋯Gd distances (Gd₁⋯G_d2, Gd₁⋯Gd₃ and Gd₁⋯Gd₄); b) tabulated measurements of distances taken from models generated with Avogadro ^[12] and c) five pulse RIDME trace (black), fit (red) and background (blue) determined by neural network analysis of Gd‐1 after storing at −80 °C, measured at Q‐band (33.62 GHz), at a temperature of 5 K with T _mix=100 μs, d) Corresponding distance distribution with 95 % confidence interval shown as the blue shaded region, with the maxima of each peak of the distribution annotated.