Table 2.
1H (150 MHz) and 13C (600 MHz) NMR data of compounds 1–3 recorded in CD3OD (δ in ppm; J in Hz).
| Pos. | 1 | 2 | 3 | |||
|---|---|---|---|---|---|---|
| δ H | δ C | δ H | δ C | δ H | δ C | |
| 2 | – | 157.3 | – | 157.5 | – | 157.4 |
| 3 | – | 160.9 | – | 161.0 | – | 161.5 |
| 5 | – | 131.3 | – | 132.8 | – | 132.8 |
| 6 | – | 135.8 | – | 135.3 | – | 134.2 |
| 7 | 3.34 m | 30.9 | 3.33 m | 31.5 | 3.33 m | 30.9 |
| 8 | 1.20 d 6.8 | 20.5 | 1.22 d 6.8 | 20.5 | 1.20 d 6.8 | 20.4 |
| 9 | 1.20 d 6.8 | 20.5 | 1.22 d 6.8 | 20.5 | 1.20 d 6.8 | 20.5 |
| 10 | 2.22 s | 15.2 | 2.29 s | 14.8 | 2.29 s | 14.8 |
| 11 | 2.57 q 7.5 | 26.1 | 4.89 q 6.5 | 66.6 | 4.52 q 6.5 | 76.6 |
| 12 | 1.17 t 7.5 | 13.7 | 1.44 d 6.5 | 22.5 | 1.47 t 6.5 | 19.5 |
| 11-OCH3 | – | – | – | – | 3.22 s | 55.9 |