Table 5.
The results of accuracy and precision for cefquinome in milk at four distinct spiked concentrations. (day = 5, n = 30).
| Spiked concentration (ng/g) | Average recovery (%) | SD (%) | Intra-day RSD (%) | Inter-day RSD (%) | ||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 | 2 | 3 | 4 | 5 | 1 | 2 | 3 | 4 | 5 | |||
| 0.2 | 97.90 | 95.08 | 98.75 | 99.21 | 98.62 | 5.83 | 3.61 | 9.97 | 4.40 | 6.57 | 4.55 | 5.95 |
| 10 | 94.97 | 100.00 | 104.93 | 99.32 | 100.48 | 5.16 | 4.98 | 2.89 | 6.65 | 2.87 | 2.59 | 5.17 |
| 20 | 94.08 | 97.08 | 97.98 | 98.96 | 99.10 | 3.73 | 2.48 | 4.26 | 3.37 | 4.99 | 2.93 | 3.95 |
| 40 | 96.99 | 97.07 | 95.92 | 98.18 | 99.38 | 3.27 | 4.25 | 4.37 | 2.03 | 2.87 | 2.66 | 3.35 |