Table 3.
Thermal parameters extracted from DSC analysis.
| Sample | 1st Heating | Cooling | 2nd Heating | ||
|---|---|---|---|---|---|
| Tg (°C) | Endothermic Peak | Tg (°C) | Tg (°C) | Endothermic Peak | |
| Bilayer | 39.6 | - | 47.5 | 53.2 | 125.5 °C * 0.444 J/g |
| Hydrophobic monolayer | 35.6 | - | 42.8 | 47.9 | - |
| Hydrophillic monolayer | - | - | - | 36.8 | 125.2 °C * 0.508 J/g |
| TM Hydrophobic | 24.1 *, (61.2) | 93.9 °C * 2.48 J/g |
41.6 | 45.6 | - |
| TM Hydrophilic | - | - | - | 35.1 | 125.6 °C * 0.683 J/g |
Parameters in parentheses indicate minor events. (*) Thermal events associated with preparation residues.